Di-tert-butyl 2-phenylhydrazine-1,1-dicarboxylate

Base Information

Chemical Name:Di-tert-butyl 2-phenylhydrazine-1,1-dicarboxylate
CAS No.:312934-59-1
Molecular Formula:C₁₆H₂₄N₂O₄
Molecular Weight:308.378
Hs Code.:
DSSTox Substance ID:DTXSID70573372
Wikidata:Q82462087
Mol file:312934-59-1.mol

Synonyms:312934-59-1;Di-tert-butyl 2-phenylhydrazine-1,1-dicarboxylate;N-Phenylhydrazine, N',N'-Bis-BOC protected;DTXSID70573372;tert-butyl N-anilino-N-[(2-methylpropan-2-yl)oxycarbonyl]carbamate

Suppliers and Price of Di-tert-butyl 2-phenylhydrazine-1,1-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-PHENYLHYDRAZINE, N',N'-BIS-BOC PROTECTED 95.00%
5MG
$ 504.81

Total 2 raw suppliers

Chemical Property of Di-tert-butyl 2-phenylhydrazine-1,1-dicarboxylate

Chemical Property:

Vapor Pressure:1.36E-05mmHg at 25°C
Boiling Point:367.5°C at 760 mmHg
PKA:1.35±0.38(Predicted)
Flash Point:176.1°C
PSA：67.87000
Density:1.134g/cm³
LogP:4.25870
XLogP3:4.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:308.17360725
Heavy Atom Count:22
Complexity:362

Purity/Quality:

99% ^*data from raw suppliers

N-PHENYLHYDRAZINE, N',N'-BIS-BOC PROTECTED 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)N(C(=O)OC(C)(C)C)NC1=CC=CC=C1

Technology Process of Di-tert-butyl 2-phenylhydrazine-1,1-dicarboxylate

There total 3 articles about Di-tert-butyl 2-phenylhydrazine-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 42116-43-8
tert-butyl 2-phenylhydrazine-1-carboxylate

: 312934-59-1
2,2-Bis(t-butyloxycarbonyl)-1-phenylhydrazine

: 312934-60-4
1,1,2-tris(tert-butoxycarbonyl)-2-phenylhydrazine

Guidance literature:: With dmap; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1055/s-2000-7600

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 312934-59-1
2,2-Bis(t-butyloxycarbonyl)-1-phenylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 0.5 h

2: 0.86 g / DMAP / acetonitrile / 3 h / 20 °C

With dmap; In acetonitrile; 1: Acylation / 2: Acylation;
DOI:10.1055/s-2000-7600

Reference yield:

: 100-63-0
phenylhydrazine

: 312934-59-1
2,2-Bis(t-butyloxycarbonyl)-1-phenylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 0.5 h

2: 0.86 g / DMAP / acetonitrile / 3 h / 20 °C

With dmap; In acetonitrile; 1: Acylation / 2: Acylation;
DOI:10.1055/s-2000-7600