7,4'-Di-O-Methylapigenin 5-O-xylosylglucoside

Base Information

Chemical Name:7,4'-Di-O-Methylapigenin 5-O-xylosylglucoside
CAS No.:221257-06-3
Molecular Formula:C28H32O14
Molecular Weight:592.54528
Hs Code.:
Mol file:221257-06-3.mol

Synonyms:7,4'-Di-O-Methylapigenin 5-O-xylosylglucoside;7-Methoxy-2-(4-methoxyphenyl)-5-[(6-O-beta-D-xylopyranosyl-beta-D-glucopyranosyl)oxy]-4H-1-benzopyran-4-one

Suppliers and Price of 7,4'-Di-O-Methylapigenin 5-O-xylosylglucoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
7,4'-Di-O-methylapigenin5-O-xylosylglucoside 95+%
5mg
$ 860.00

Arctom
7,4'-Di-O-methylapigenin5-O-xylosylglucoside
5mg
$ 553.00

Total 9 raw suppliers

Chemical Property of 7,4'-Di-O-Methylapigenin 5-O-xylosylglucoside

Chemical Property:

PSA：206.97000
LogP:-0.88080

Purity/Quality:

98% ^*data from raw suppliers

7,4'-Di-O-methylapigenin5-O-xylosylglucoside 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 7,4'-Di-O-Methylapigenin 5-O-xylosylglucoside

There total 10 articles about 7,4'-Di-O-Methylapigenin 5-O-xylosylglucoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 5-O-(2′′′,3′′′,4′′′-tri-O-benzoyl-β-D-xylopyranosyl(1→6)-2″,3″,4″-tri-O-acetyl-β-D-glucopyranosyl)-7,4′-di-O-methylapigenin

: 221257-06-3
7,4'-di-O-methylapigenin 5-O-1-β-xylopyranosyl(1->6)-β-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 72h; pH=10;
DOI:10.1039/c7ob01004d

Reference yield:

: 29424-96-2,102101-05-3,120851-84-5,137329-43-2,13238-06-7
naringenin-4',7-dimethyl ether

: 221257-06-3
7,4'-di-O-methylapigenin 5-O-1-β-xylopyranosyl(1->6)-β-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: dmap; triethylamine / dichloromethane / 0.17 h / 20 °C

2: sodium tetrahydroborate / tetrahydrofuran; water / 0 °C

3: 2,6-di-tert-butyl-4-methylpyridine; boron trifluoride diethyl etherate / dichloromethane / 3.5 h / 20 °C

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 20 h / 20 °C

5: sodium methylate / methanol; dichloromethane / 72 h / 20 °C / pH 10

With dmap; sodium tetrahydroborate; 2,6-di-tert-butyl-4-methylpyridine; boron trifluoride diethyl etherate; sodium methylate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c7ob01004d

Reference yield:

: 81148-82-5
5-acetoxy-7,4′-dimethoxyflavanone

: 221257-06-3
7,4'-di-O-methylapigenin 5-O-1-β-xylopyranosyl(1->6)-β-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / tetrahydrofuran; water / 0 °C

2: 2,6-di-tert-butyl-4-methylpyridine; boron trifluoride diethyl etherate / dichloromethane / 3.5 h / 20 °C

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 20 h / 20 °C

4: sodium methylate / methanol; dichloromethane / 72 h / 20 °C / pH 10

With sodium tetrahydroborate; 2,6-di-tert-butyl-4-methylpyridine; boron trifluoride diethyl etherate; sodium methylate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c7ob01004d