17-Oxo-6,9,12-trioxa-2,16-diazaeicosanedioic acid 1-(1,1-dimethylethyl)ester

Base Information

Chemical Name:17-Oxo-6,9,12-trioxa-2,16-diazaeicosanedioic acid 1-(1,1-dimethylethyl)ester
CAS No.:250612-31-8
Molecular Formula:C19H36N2O8
Molecular Weight:420.503
Hs Code.:
Mol file:250612-31-8.mol

Synonyms:17-Oxo-6,9,12-trioxa-2,16-diazaeicosanedioic acid 1-(1,1-dimethylethyl)ester;N-Boc-Nμ-succinyl-4,7,10-trioxa-1,13-tridecanediamine;N-Boc-N'-succinyl-4,7,10-trioxa-1,13-tridecanediamine 95% (HPLC)

Suppliers and Price of 17-Oxo-6,9,12-trioxa-2,16-diazaeicosanedioic acid 1-(1,1-dimethylethyl)ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N-Boc-N′-succinyl-4,7,10-trioxa-1,13-tridecanediamine 95% (HPLC)
1g
$ 186.00

Sigma-Aldrich
N-Boc-N′-succinyl-4,7,10-trioxa-1,13-tridecanediamine 95% (HPLC)
5g
$ 676.00

American Custom Chemicals Corporation
N-BOC-N'-SUCCINYL-4,7,10-TRIOXA-1,13-TRIDECANEDIAMINE 95.00%
5G
$ 1388.00

American Custom Chemicals Corporation
N-BOC-N'-SUCCINYL-4,7,10-TRIOXA-1,13-TRIDECANEDIAMINE 95.00%
1G
$ 756.15

Adipogen Life Sciences
N-Boc-N'-succinyl-4,7,10-trioxa-1,13-tridecanediamine ≥95%(HPLC)
2.5 g
$ 212.00

Total 7 raw suppliers

Chemical Property of 17-Oxo-6,9,12-trioxa-2,16-diazaeicosanedioic acid 1-(1,1-dimethylethyl)ester

Chemical Property:

PSA：139.40000
LogP:2.36680
Storage Temp.:?20°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-Boc-N′-succinyl-4,7,10-trioxa-1,13-tridecanediamine 95% (HPLC) ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 22

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 17-Oxo-6,9,12-trioxa-2,16-diazaeicosanedioic acid 1-(1,1-dimethylethyl)ester

There total 4 articles about 17-Oxo-6,9,12-trioxa-2,16-diazaeicosanedioic acid 1-(1,1-dimethylethyl)ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: benzyl 2,2-dimethyl-4,20-dioxo-3,9,12,15-tetraoxa-5,19-diazatricosan-23-oate

: 250612-31-8
3-(N-(3-(2-(2-(3-((tert-butoxy)-carbonylamino)propoxy)ethoxy)ethoxy)propyl)carbamoyl)-propanoic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2013.08.065

Reference yield: 91.0%

: 108-30-5
succinic acid anhydride

: 194920-62-2
tert-butyl N-(3-{2-[2-(3-aminopropoxy)ethoxy]ethoxy}propyl)carbamate

: 250612-31-8
3-(N-(3-(2-(2-(3-((tert-butoxy)-carbonylamino)propoxy)ethoxy)ethoxy)propyl)carbamoyl)-propanoic acid

Guidance literature:: With pyridine; In dichloromethane; acetonitrile; at 20 ℃; for 3.5h;
DOI:10.1021/ja026917a

Reference yield:

: 4246-51-9
4,7,10-trioxa-1,13-diaminotridecane

: 250612-31-8
3-(N-(3-(2-(2-(3-((tert-butoxy)-carbonylamino)propoxy)ethoxy)ethoxy)propyl)carbamoyl)-propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N / CH₂Cl₂ / 4 h / 20 °C

2: 91 percent / pyridine / CH₂Cl₂; acetonitrile / 3.5 h / 20 °C

With pyridine; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/ja026917a