4,9-Dibromo-2,7-bis(3-(dimethylamino)propyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone

Base Information

Chemical Name:4,9-Dibromo-2,7-bis(3-(dimethylamino)propyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone
CAS No.:1375748-41-6
Molecular Formula:C₂₄H₂₆Br₂N₄O₄
Molecular Weight:594.303
Hs Code.:
Mol file:1375748-41-6.mol

Synonyms:4,9-Dibromo-2,7-bis(3-(dimethylamino)propyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone

Suppliers and Price of 4,9-Dibromo-2,7-bis(3-(dimethylamino)propyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 7 raw suppliers

Chemical Property of 4,9-Dibromo-2,7-bis(3-(dimethylamino)propyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

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Technology Process of 4,9-Dibromo-2,7-bis(3-(dimethylamino)propyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone

There total 3 articles about 4,9-Dibromo-2,7-bis(3-(dimethylamino)propyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 83204-68-6
2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid dianhydride

: 109-55-7
1-amino-3-(dimethylamino)propane

: 1375748-41-6
4,9-dibromo-2,7-bis[3-(dimethylamino)propyl]-benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone

Guidance literature:: In acetic acid; at 130 ℃; for 0.5h;
DOI:10.1039/c2ob07006e

Reference yield: 35.0%

: 1029434-09-0
2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid

: 109-55-7
1-amino-3-(dimethylamino)propane

: 1375748-41-6
4,9-dibromo-2,7-bis[3-(dimethylamino)propyl]-benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone

: C₂₄H₂₇BrN₄O₄

Guidance literature:: In acetic acid; at 120 ℃; for 0.5h;
DOI:10.3390/ijms21061964

Reference yield:

: 81-30-1
1,4,5,8-naphthalenetetracarboxylic dianhydride

: 1375748-41-6
4,9-dibromo-2,7-bis[3-(dimethylamino)propyl]-benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone

Guidance literature:: Multi-step reaction with 2 steps

1: carbromal; sulfuric acid / 72 h / 50 °C

2: acetic acid / 5 h / 120 °C

With carbromal; sulfuric acid; acetic acid;
DOI:10.1039/c9tc00721k