BENZENEETHANIMIDAMIDE, 3-BROMO-N-HYDROXY-4-METHOXY

Base Information

• Chemical Name: BENZENEETHANIMIDAMIDE, 3-BROMO-N-HYDROXY-4-METHOXY
• CAS No.: 777-64-0
• Molecular Formula: C9H11BrN2O2
• Molecular Weight: 0
• Mol file: 777-64-0.mol

Synonyms:BENZENEETHANIMIDAMIDE, 3-BROMO-N-HYDROXY-4-METHOXY

Chemical Property of BENZENEETHANIMIDAMIDE, 3-BROMO-N-HYDROXY-4-METHOXY

Chemical Property:

• PSA: 67.84000
• LogP: 2.44690

Purity/Quality:

BENZENEETHANIMIDAMIDE,3-BROMO-N-HYDROXY-4-METHOXY 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZENEETHANIMIDAMIDE, 3-BROMO-N-HYDROXY-4-METHOXY

There total 2 articles about BENZENEETHANIMIDAMIDE, 3-BROMO-N-HYDROXY-4-METHOXY which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3-bromo-4-methoxyphenyl)-acetonitrile (772-59-8) → 2-(3-Bromo-4-methoxy-phenyl)-N-hydroxy-acetamidine (777-64-0)

Guidance literature:

With hydroxylamine hydrochloride; potassium hydroxide; In methanol; at 60 ℃; for 17h;

DOI:10.1021/jm900597q

Reference yield:

→ 2-(3-Bromo-4-methoxy-phenyl)-N-hydroxy-acetamidine (777-64-0)

Guidance literature:

entspr. Nitril, Hydroxylamin;

Reference yield:

2-(3-Bromo-4-methoxy-phenyl)-N-hydroxy-acetamidine (777-64-0) + dimethyl acetylenedicarboxylate (762-42-5) → C15H17BrN2O6

Guidance literature:

In chloroform; at 60 ℃; for 1h;

DOI:10.1021/jm900597q

upstream raw materials:

(3-bromo-4-methoxyphenyl)-acetonitrile

Refernces