5-Nitro-1-(2-O,3-O,4-O,6-O-tetraacetyl-β-D-glucopyranosyl)-1H-indole

Base Information

Chemical Name:5-Nitro-1-(2-O,3-O,4-O,6-O-tetraacetyl-β-D-glucopyranosyl)-1H-indole
CAS No.:29742-55-0
Molecular Formula:C₂₂H₂₄N₂O₁₁
Molecular Weight:492.439
Hs Code.:
Mol file:29742-55-0.mol

Synonyms:5-Nitro-1-(2-O,3-O,4-O,6-O-tetraacetyl-β-D-glucopyranosyl)-1H-indole

Suppliers and Price of 5-Nitro-1-(2-O,3-O,4-O,6-O-tetraacetyl-β-D-glucopyranosyl)-1H-indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 5-Nitro-1-(2-O,3-O,4-O,6-O-tetraacetyl-β-D-glucopyranosyl)-1H-indole

Chemical Property:

Melting Point:163 °C
PSA：165.18000
LogP:2.32830

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 5-Nitro-1-(2-O,3-O,4-O,6-O-tetraacetyl-β-D-glucopyranosyl)-1H-indole

There total 5 articles about 5-Nitro-1-(2-O,3-O,4-O,6-O-tetraacetyl-β-D-glucopyranosyl)-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 26386-09-4
1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-nitroindoline

: 29742-55-0
1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-nitroindole

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; at 100 ℃; for 72h;
DOI:10.1016/j.ejmech.2005.10.004

Reference yield:

: 32692-19-6
5-nitro-2,3-dihydro-1H-indole

: 29742-55-0
1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-nitroindole

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / ethanol; H₂O / 144 h / 90 °C

2: 78 percent / pyridine / 24 h / 20 °C

3: 98 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / dioxane / 72 h / 100 °C

With pyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; ethanol; water;
DOI:10.1016/j.ejmech.2005.10.004

Reference yield:

: 50-99-7
D-glucose

: 29742-55-0
1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-nitroindole

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / ethanol; H₂O / 144 h / 90 °C

2: 78 percent / pyridine / 24 h / 20 °C

3: 98 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / dioxane / 72 h / 100 °C

With pyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; ethanol; water;
DOI:10.1016/j.ejmech.2005.10.004