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D(+)-Glucose 50-99-7 TOP supplier in China
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USD $ 12.0-13.0 / Kilogram 1 Kilogram 1-10 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
D(+)-Glucose 50-99-7
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No Data 1 Kilogram 10000 Metric Ton/Month Shanghai Upbio Tech Co.,Ltd Contact Supplier
D(+)-Glucose
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USD $ 1.0-1.0 / Kilogram 5 Kilogram 10000 Metric Ton/Year Chemwill Asia Co., Ltd. Contact Supplier
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USD $ 6.0-12.0 / Gram 50 Gram 100000 Kilogram/Day WUHAN MULEI NEW MATERIAL CO., LTD Contact Supplier
D-GLUCOSE chemical Organic Intermediate CAS No.: 50-99-7
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USD $ 3.0-3.0 / Gram 1 Gram 10 Metric Ton/Month Hebei yanxi chemical co.,LTD. Contact Supplier
Best price ,high quality ,Dextrose anhydrous
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D-(+)-Glucose
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Factory of Dextrose anhydrous
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USD $ 6.0-8.0 / Kilogram 25 Kilogram 1000 Metric Ton/Month EAST CHEMSOURCES LIMITED Contact Supplier
Dextrose anhydrous
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50-99-7 Usage

Health Hazard

No toxicity

Brand name

Cartose (Sterling Winthrop) Dextrose.

Description

D(+)-glucose ,a short form of dextrorotatory glucose, is a stereoisomer of glucose molecule, which is biologically active and whose bottom chiral carbon has its hydroxyl group (OH) located spatially to the right. Its molecule can exist in an open-chain (acyclic) and ring (cyclic) form and has two isomers α- and β-. It is the main source of energy in the form of ATP for living organisms. It is naturally occurring and is found in fruits and other parts of plants in its free state. In animals, it arises from the breakdown of glycogen in a process known as glycogenolysis. D-(+)-Glucose has been used as a standard for the estimation of total sugar in hydrolyzed starch by phenol-sulfuric acid method. It has also been used in the preparation of the liquid media for culturing some yeast cells. In addition, it is used therapeutically in fluid and nutrient replacement, such as glucose syrup and glucose powder. It can be obtained by enzymatic cleavage of starch, so there are multiple sources like sugar cane, sugar beet, corn (corn syrup), potatoes and wheat. Today, large-scale starch hydrolysis is used to produce glucose.

Purification Methods

Crystallise -D-glucose from hot glacial acetic acid or pyridine. Traces of solvent are removed by drying in a vacuum oven at 75o for >3hours. [Gottfried Adv Carbohydr Chem 5 127 1950, Kjaer & Lindberg Acta Chem Scand 1 3 1713 1959, Whistler & Miller Methods in Carbohydrate Chemistry I 1301962, Academic Press, Beilstein 1 IV 4306.] [For equilibrium forms see Angyal Adv Carbohydr Chem 42 15 1984, Angyal & Pickles Aust J Chem 25 1711 1972.]

References

1. http://www.sigmaaldrich.com/catalog/product/sigma/g8270?lang=en&region=CA
2. https://pubchem.ncbi.nlm.nih.gov/compound/D-glucose#section=Top
3. http://www.hmdb.ca/metabolites/HMDB00122
4. http://www.biology-online.org/dictionary/D-glucose
5. http://www3.hhu.de/biodidaktik/zucker/sugar/glukose.html

Reactivity Profile

A weak reducing agent.

Definition

ChEBI: The open chain form of D-glucose.

Air & Water Reactions

Water soluble.

Uses

Dextrose(D-glucose), a simple sugar (monosaccharide), is an important carbohydrate in biology

Uses

A primary source of energy for living organisms

Chemical Properties

White crystalline powder

General Description

Watery odorless colorless liquid. Denser than water and soluble in water. Hence sinks in and mixes with water.

Uses

Labelled D-Glucose is a simple sugar that is present in plants. A monosaccharide that may exist in open chain or cyclic conformation if in solution. It plays a vital role in photosynthesis and fuels the energy required for cellular respiration. D-Glucose is used in various metabolic processes including enzymic synthesis of cyclohexyl-α and β-D-glucosides. Can also be used as a diagnostic tool in detection of type 2 diabetes mellitus and potentially Huntington's disease through analysis of blood-glucose in type 1 diabetes mellitus.
InChI:InChI=1/C6H12O6/c7-1-3(9)5(11)6(12)4(10)2-8/h1,3-6,8-12H,2H2/t3-,4+,5+,6+/m0/s1

50-99-7 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Supelco (47249)  D-(+)-Glucose  analytical standard 50-99-7 000000000000047249 312.39CNY Detail
Sigma-Aldrich (49152)  D-(+)-Glucose  tested according to Ph.Eur., anhydrous 50-99-7 49152-1KG 1,434.42CNY Detail
Sigma-Aldrich (16325)  D-(+)-Glucose  meets analytical specification of Ph. Eur., BP, anhydrous 50-99-7 16325-1KG 627.12CNY Detail
Sigma-Aldrich (G5767)  D-(+)-Glucose  ACS reagent 50-99-7 G5767-5KG 2,182.05CNY Detail
Sigma-Aldrich (G5767)  D-(+)-Glucose  ACS reagent 50-99-7 G5767-500G 457.47CNY Detail
Sigma-Aldrich (G5767)  D-(+)-Glucose  ACS reagent 50-99-7 G5767-25G 325.26CNY Detail
USP (1181302)  Dextrose  United States Pharmacopeia (USP) Reference Standard 50-99-7 1181302-500MG 4,662.45CNY Detail
Sigma-Aldrich (PHR1000)  D-(+)-Glucose  pharmaceutical secondary standard; traceable to USP and PhEur 50-99-7 PHR1000-1G 732.19CNY Detail
Supelco (47829)  D-(+)Glucose  analytical standard 50-99-7 000000000000047829 376.74CNY Detail
Alfa Aesar (A16828)  D-(+)-Glucose, anhydrous, 99%    50-99-7 10000g 2295.0CNY Detail
Alfa Aesar (A16828)  D-(+)-Glucose, anhydrous, 99%    50-99-7 2500g 714.0CNY Detail
Alfa Aesar (A16828)  D-(+)-Glucose, anhydrous, 99%    50-99-7 500g 245.0CNY Detail

50-99-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 11, 2017

Revision Date: Aug 11, 2017

1.Identification

1.1 GHS Product identifier

Product name aldehydo-D-glucose

1.2 Other means of identification

Product number -
Other names D-(+)-Glucose

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Processing Aids and Additives
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:50-99-7 SDS

50-99-7Synthetic route

cellulose

cellulose

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
With lithium chloride In N,N-dimethyl-formamide at 120℃; for 8h; Catalytic behavior; Reagent/catalyst; Temperature; Solvent;99%
With hydrogenchloride; water for 3h; Reactivity; Ionic liquid;94%
Tonsil Supreme 110F, impregnated gallium sulphate In water at 20 - 110℃; for 0.35h; Product distribution / selectivity;75%
1,2-O-benzylidene-α-D-glucofuranose
22154-74-1

1,2-O-benzylidene-α-D-glucofuranose

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
With ammonium formate; palladium on activated charcoal In methanol for 0.666667h; Product distribution; Heating; at various types of sugars;97%
Cellobiose
13360-52-6

Cellobiose

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
With water at 120℃; for 1h; Autoclave;96%
With sulfuric acid In water at 130℃; for 6h; pH=4; Kinetics; Catalytic behavior; pH-value; Temperature; Inert atmosphere; Sealed tube;91.1%
With phosphotungstic acid hydrate; water at 160℃; for 0.5h; Reagent/catalyst; Temperature;37.6%
ptaquiloside
87625-62-5

ptaquiloside

A

D-glucose
50-99-7

D-glucose

B

C14H18O2
87701-34-6

C14H18O2

Conditions
ConditionsYield
With sodium carbonate In water at 25℃; for 0.333333h; pH:8-11;A n/a
B 95%
With glycosidase Inert atmosphere; Enzymatic reaction;
amylose

amylose

amylopectin

amylopectin

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
With water at 150℃; for 3h; Autoclave;95%
cellulose

cellulose

A

5-hydroxymethyl-2-furfuraldehyde
67-47-0

5-hydroxymethyl-2-furfuraldehyde

B

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
With hydrogenchloride; water for 4h; Reactivity; Ionic liquid;A 6%
B 93%
With carbon based mesoporous Sibunit-4-ox In water for 5h;A n/a
B 45%
With water; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride at 160℃; for 2.66667h; Product distribution / selectivity;A 7%
B 32%
(2S,3R)-3,7-dimethyl-6-octene-1,2,3-triol 2-O-β-D-glucopyranoside

(2S,3R)-3,7-dimethyl-6-octene-1,2,3-triol 2-O-β-D-glucopyranoside

A

D-glucose
50-99-7

D-glucose

B

(2S,3R)-3,7-dimethyl-6-octene-1,2,3-triol
90988-60-6

(2S,3R)-3,7-dimethyl-6-octene-1,2,3-triol

Conditions
ConditionsYield
With β-glucosidase In water at 37℃; for 96h; Enzymatic reaction;A n/a
B 93%
protogenkwanin-4'-glucoside
78983-46-7

protogenkwanin-4'-glucoside

A

D-glucose
50-99-7

D-glucose

B

protogenkwanin
74996-29-5

protogenkwanin

Conditions
ConditionsYield
With cellulase from Aspergillus niger at 40℃; for 144h; pH=4.6;A n/a
B 92%
cellobiose
528-50-7

cellobiose

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
In water at 249℃; for 0.0166667h; Product distribution; Kinetics; Thermodynamic data; activation energy; various pH (3-5.7), temperatures (180-249 deg C), and times (0.3-15 min);90%
With recombinant C,N-terminal 6xHis-tagged rabbit cecum umbgl3B β-glucosidase; water at 28℃; for 0.25h; pH=6; aq. phosphate buffer;
With Bgl1T β-D-glucoside glucohydrolase; calcium chloride at 37℃; for 0.25h; pH=7; aq. phosphate buffer; Enzymatic reaction;
cellulose

cellulose

A

D-glucose
50-99-7

D-glucose

B

levulinic acid
123-76-2

levulinic acid

Conditions
ConditionsYield
With dodecatungstophosphoric acid hydrate; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride In water at 139.84℃; for 5h; Reagent/catalyst;A 89%
B n/a
With water at 150℃; for 12h; Autoclave;A 12%
B 42%
With 1-(3-sulfopropyl)pyridinium phosphotungstate; water at 150℃; under 15001.5 Torr; for 5h; Autoclave; Inert atmosphere;A 32.9%
B 18.1%
12β-O-acetyl-3-O-(β-D-glucopyranosyl-(1→4)-6-deoxy-3-O-methyl-β-D-allopyranosyl-(1→4)-D-oleandronyl)-11α-O-tigloyltenacigenin B

12β-O-acetyl-3-O-(β-D-glucopyranosyl-(1→4)-6-deoxy-3-O-methyl-β-D-allopyranosyl-(1→4)-D-oleandronyl)-11α-O-tigloyltenacigenin B

A

D-glucose
50-99-7

D-glucose

B

12β-O-acetyl-3-O-(6-deoxy-3-O-methyl-β-D-allopyranosyl-(1→4)-D-oleandronyl)-11α-O-tigloyltenacigenin B

12β-O-acetyl-3-O-(6-deoxy-3-O-methyl-β-D-allopyranosyl-(1→4)-D-oleandronyl)-11α-O-tigloyltenacigenin B

Conditions
ConditionsYield
With cellulase In aq. acetate buffer at 37℃; for 168h; pH=5; Enzymatic reaction;A 88%
B 4 mg
(3S,4R,5S,7R,9S)-megastigma-6,7-diene-3,4,5,9-tetrol 4-O-β-D-glucopyranoside

(3S,4R,5S,7R,9S)-megastigma-6,7-diene-3,4,5,9-tetrol 4-O-β-D-glucopyranoside

A

D-glucose
50-99-7

D-glucose

B

crotalionol A

crotalionol A

Conditions
ConditionsYield
With hesperidinase; emulsin; water at 37℃; for 24h;A 86%
B 72%
megastigman-7-en-3,6-epoxy-5,9-diol 9-O-β-D-glucopyranoside
1374460-70-4

megastigman-7-en-3,6-epoxy-5,9-diol 9-O-β-D-glucopyranoside

A

D-glucose
50-99-7

D-glucose

crotalionol C

crotalionol C

Conditions
ConditionsYield
With hesperidinase; emulsin; water at 37℃; for 24h;A 67%
B 86%
Sucrose
57-50-1

Sucrose

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
With water at 79.84℃; for 2h;85.9%
With water; acetone in Gegenwart eines sauren Kationenaustauschers;
With potassium phosphate buffer; rat intestinal α-glucosidase; 5,6,7-trihydroxy-2-phenyl-4H-1-benzopyran-4-one In dimethyl sulfoxide at 37℃; for 0.25h; pH=6.3; Enzyme kinetics;
(3R,4R,5S,6S,7E,9R)-megastigman-7-ene-3,4,9-triol 9-O-β-D-glucopyranoside
1232683-60-1

(3R,4R,5S,6S,7E,9R)-megastigman-7-ene-3,4,9-triol 9-O-β-D-glucopyranoside

A

D-glucose
50-99-7

D-glucose

B

(3R,4R,5S,6S,7E,9R)-megastigman-7-ene-3,4,9-triol

(3R,4R,5S,6S,7E,9R)-megastigman-7-ene-3,4,9-triol

Conditions
ConditionsYield
With hesperidinase; emulsin; water at 37℃; for 18h; Enzymatic reaction;A 85%
B 76%
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose
582-52-5

1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
With K 10 clay In methanol; water at 75℃; for 72h;83%
2,3,4,5,6-penta-O-benzyl aldehydo D-glucose
78699-85-1

2,3,4,5,6-penta-O-benzyl aldehydo D-glucose

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
With hydrogen; palladium dihydroxide In methanol for 120h; Ambient temperature;83%
alpha-D-glucopyranose
492-62-6

alpha-D-glucopyranose

1-amino-2-propene
107-11-9

1-amino-2-propene

A

D-glucose
50-99-7

D-glucose

B

1-(allylamino)-1-deoxy-β-D-glucopyranose

1-(allylamino)-1-deoxy-β-D-glucopyranose

Conditions
ConditionsYield
In ethanol at 53℃; for 1h; Temperature; Time; Inert atmosphere;A n/a
B 81.4%
starch

starch

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
With H3N*2H(1+)*TeW6O21(2-); water at 130℃; for 4h; Autoclave;78.4%
With Arthrobacter sp. DL001 α-D-glucoside glucohydrolase; water at 30℃; for 0.5h; pH=5.5; citrate-phosphate buffer; Enzymatic reaction;
(3S,4R,5S,7R,9R)-megastigma-6,7-diene-3,4,5,9-tetrol 4-O-β-D-glucopyranoside

(3S,4R,5S,7R,9R)-megastigma-6,7-diene-3,4,5,9-tetrol 4-O-β-D-glucopyranoside

A

D-glucose
50-99-7

D-glucose

B

crotalionol B

crotalionol B

Conditions
ConditionsYield
With hesperidinase; emulsin; water at 37℃; for 24h;A 50%
B 74%
(2S)-naringenin 5-O-β-D-glucopyranosyl(1->6)-β-D-glucopyranoside
1160434-44-5

(2S)-naringenin 5-O-β-D-glucopyranosyl(1->6)-β-D-glucopyranoside

A

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
With hydrogenchloride; water at 80℃; for 1h;A n/a
B 73%
(2R)-naringenin 5-O-β-D-glucopyranosyl(1->6)-β-D-glucopyranoside

(2R)-naringenin 5-O-β-D-glucopyranosyl(1->6)-β-D-glucopyranoside

A

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
With hydrogenchloride; water at 80℃; for 1h;A n/a
B 73%
microcrystalline cellulose

microcrystalline cellulose

A

5-hydroxymethyl-2-furfuraldehyde
67-47-0

5-hydroxymethyl-2-furfuraldehyde

B

formic acid
64-18-6

formic acid

C

D-glucose
50-99-7

D-glucose

D

levulinic acid
123-76-2

levulinic acid

Conditions
ConditionsYield
With graphene oxide (GO) In water at 199.84℃; for 1h; Temperature; Microwave irradiation; Green chemistry;A n/a
B n/a
C 73%
D n/a
chalconaringenin 2'-O-β-D-glucopyranosyl(1->6)-β-D-glucopyranoside

chalconaringenin 2'-O-β-D-glucopyranosyl(1->6)-β-D-glucopyranoside

A

D-glucose
50-99-7

D-glucose

B

2',4',6',4-tetrahydroxydihydrochalcone
25515-46-2, 73692-50-9

2',4',6',4-tetrahydroxydihydrochalcone

Conditions
ConditionsYield
With hydrogenchloride; water at 80℃; for 1h;A n/a
B 72%
D-glucose
50-99-7

D-glucose

D-sorbitol
50-70-4

D-sorbitol

Conditions
ConditionsYield
With hydrogen In water at 120℃; under 15001.5 Torr; for 1h;100%
With hydrogen; ruthenium embedded in mesoporous carbon In water at 120℃; under 15001.5 Torr; for 2h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Autoclave;99.3%
With hydrogen at 120℃; under 22502.3 Torr; for 2h; high pressure reactor;94.43%
D-glucose
50-99-7

D-glucose

3,4-di-O-formyl-D-erythrose

3,4-di-O-formyl-D-erythrose

Conditions
ConditionsYield
With lead(IV) acetate In acetic acid at 16 - 28℃; for 0.75h; oxidative cleavage;100%
D-glucose
50-99-7

D-glucose

O-(4-methoxybenzyl)-hydroxylamine HCl

O-(4-methoxybenzyl)-hydroxylamine HCl

(2S,3R,4R,5R)-2,3,4,5,6-Pentahydroxy-hexanal O-(4-methoxy-benzyl)-oxime
365278-77-9

(2S,3R,4R,5R)-2,3,4,5,6-Pentahydroxy-hexanal O-(4-methoxy-benzyl)-oxime

Conditions
ConditionsYield
In acetate buffer at 20℃; for 2.16667h; pH=4;100%
D-glucose
50-99-7

D-glucose

7-hydroxy-8-hydroxyaminomethylcoumarin
365278-56-4

7-hydroxy-8-hydroxyaminomethylcoumarin

C16H19NO9

C16H19NO9

Conditions
ConditionsYield
In phosphate buffer at 20℃; pH=6.5;100%
D-glucose
50-99-7

D-glucose

N-(3-methoxybenzyl)hydroxylamine hydrochloride

N-(3-methoxybenzyl)hydroxylamine hydrochloride

C14H21NO7

C14H21NO7

Conditions
ConditionsYield
In phosphate buffer at 20℃; pH=6.5;100%
D-glucose
50-99-7

D-glucose

8-aminooxymethyl-7-hydroxycoumarin

8-aminooxymethyl-7-hydroxycoumarin

2,3,4,5,6-pentahydroxy-hexanal O-(7-hydroxy-2-oxo-2H-chromen-8-ylmethyl)-oxime

2,3,4,5,6-pentahydroxy-hexanal O-(7-hydroxy-2-oxo-2H-chromen-8-ylmethyl)-oxime

Conditions
ConditionsYield
In acetate buffer at 20℃; for 2.16667h; pH=4;100%
D-glucose
50-99-7

D-glucose

ethanamine hydrochloride
557-66-4

ethanamine hydrochloride

N-ethyl-D-gluconamide

N-ethyl-D-gluconamide

Conditions
ConditionsYield
With iodine; potassium carbonate In methanol at 20℃; for 6h;100%
D-glucose
50-99-7

D-glucose

ethanol
64-17-5

ethanol

Conditions
ConditionsYield
With manganese(II) sulfate; rubidium sulfate; sulfuric acid; magnesium sulfate In water at 40℃; for 0.166667h; Temperature; Reagent/catalyst;100%
With cesium sulfate; sulfuric acid; water; magnesium sulfate; 2Co(2+)*2O4S(2-) at 145℃;
With sulfuric acid In water at 33℃; for 72h; pH=3.9; Kinetics; Reagent/catalyst; Temperature; Microbiological reaction;
2-[2-(vinyloxy)ethoxymethyl]oxirane
16801-19-7

2-[2-(vinyloxy)ethoxymethyl]oxirane

D-glucose
50-99-7

D-glucose

1,2,3,5,6-penta-O-{1-[2-(glycidyloxy)ethoxy]ethyl}-D-glucopyranose

1,2,3,5,6-penta-O-{1-[2-(glycidyloxy)ethoxy]ethyl}-D-glucopyranose

Conditions
ConditionsYield
With trifluoroacetic acid at 100 - 110℃; for 1h; Temperature;100%
D-glucose
50-99-7

D-glucose

3-dibutylaminopropylamine
102-83-0

3-dibutylaminopropylamine

C17H36N2O5

C17H36N2O5

Conditions
ConditionsYield
In methanol; water at 65℃; for 0.166667h; Schiff Reaction; Inert atmosphere;100%
In neat (no solvent) at 25℃; for 24h; Kinetics; Solvent;
methanol
67-56-1

methanol

D-glucose
50-99-7

D-glucose

Methyl formate
107-31-3

Methyl formate

Conditions
ConditionsYield
With H8[PMo7V5O40]; oxygen at 90℃; under 15001.5 Torr; for 24h; Autoclave;100%
With H8[PMo7V5O40]; oxygen at 90℃; under 15001.5 Torr; for 24h; Autoclave;
D-glucose
50-99-7

D-glucose

gluconic acid
526-95-4

gluconic acid

Conditions
ConditionsYield
With sodium carbonate In water at 30℃; for 40h; Wavelength; Irradiation;99%
With oxygen; sodium carbonate In water at 24.84℃; under 750.075 Torr; for 2h; pH=< 9; Catalytic behavior; Reagent/catalyst;99%
With 5% Pd/C; water; oxygen; sodium carbonate at 20℃; under 760.051 Torr; for 2h; Reagent/catalyst;98%
Conditions
ConditionsYield
With sodium acetate at 100℃; for 0.333333h;99%
D-glucose
50-99-7

D-glucose

butyryl chloride
141-75-3

butyryl chloride

[(2R,3R,4S,5R)-3,4,5,6-tetra(butanoyloxy)tetrahydropyran-2-yl]methyl butanoate
125161-50-4

[(2R,3R,4S,5R)-3,4,5,6-tetra(butanoyloxy)tetrahydropyran-2-yl]methyl butanoate

Conditions
ConditionsYield
Stage #1: D-glucose; butyryl chloride In dichloromethane at 15℃; for 0.5h;
Stage #2: With pyridine In dichloromethane at 15℃; for 15.5h;
98%
Stage #1: D-glucose; butyryl chloride In dichloromethane at 15℃; for 0.5h;
Stage #2: With pyridine In dichloromethane at 15℃; for 16h;
98.46%
Stage #1: D-glucose; butyryl chloride In dichloromethane at 15℃; for 0.5h;
Stage #2: With pyridine In dichloromethane at 15℃; for 16h;
98.46%
D-glucose
50-99-7

D-glucose

acetic anhydride
108-24-7

acetic anhydride

β-D-glucose pentaacetate
604-69-3

β-D-glucose pentaacetate

Conditions
ConditionsYield
Stage #1: acetic anhydride With sodium acetate for 0.333333h; Reflux;
Stage #2: D-glucose for 0.25h; Reflux;
98%
With sodium acetate at 90℃; for 4h; Inert atmosphere;85%
With sodium thiocyanide
4,5-Dichloro-1,2-phenylenediamine
5348-42-5

4,5-Dichloro-1,2-phenylenediamine

D-glucose
50-99-7

D-glucose

(1'S,2'R,3'R,4'R)-1H-2-[(1,2,3,4,5-pentahydroxy)pentyl]-5,6-dichlorobenzimidazole
108757-42-2

(1'S,2'R,3'R,4'R)-1H-2-[(1,2,3,4,5-pentahydroxy)pentyl]-5,6-dichlorobenzimidazole

Conditions
ConditionsYield
With air; iodine; acetic acid at 20℃; for 3h;98%
D-glucose
50-99-7

D-glucose

2,3-Diaminonaphthalene
771-97-1

2,3-Diaminonaphthalene

(1'S,2'R,3'R,4'R)-2-[1',2',3',4',5'-pentahydroxypentyl]-1H-naphthimidazole
1027103-22-5

(1'S,2'R,3'R,4'R)-2-[1',2',3',4',5'-pentahydroxypentyl]-1H-naphthimidazole

Conditions
ConditionsYield
With air; iodine; acetic acid at 20℃; for 6h;98%
With iodine; acetic acid at 20℃; for 6h;
D-glucose
50-99-7

D-glucose

1,2-diamino-benzene
95-54-5

1,2-diamino-benzene

(1'S,2'R,3'R,4'R)-2-[1',2',3',4',5'-pentahydroxypentyl]-1H-benzimidazole
7147-74-2

(1'S,2'R,3'R,4'R)-2-[1',2',3',4',5'-pentahydroxypentyl]-1H-benzimidazole

Conditions
ConditionsYield
With air; iodine; acetic acid at 20℃; for 8h;98%
carbonic acid bis(1-isopropylhydrazide) dihydrochloride

carbonic acid bis(1-isopropylhydrazide) dihydrochloride

D-glucose
50-99-7

D-glucose

1'S,2'R,3'R,4'R-2,4-diisopropyl-6-(1',2',3',4',5'-pentahydroxypentyl)-1,2,4,5-tetrazinan-3-one

1'S,2'R,3'R,4'R-2,4-diisopropyl-6-(1',2',3',4',5'-pentahydroxypentyl)-1,2,4,5-tetrazinan-3-one

Conditions
ConditionsYield
With sodium acetate In water at 20℃;98%
D-glucose
50-99-7

D-glucose

5,7-dihydroxy-4-phenyl-2H-1-benzopyran-2-one
7758-73-8

5,7-dihydroxy-4-phenyl-2H-1-benzopyran-2-one

6-(C-β-D-Glucosyl)-4-phenyl-5,7-dihydroxycoumarin

6-(C-β-D-Glucosyl)-4-phenyl-5,7-dihydroxycoumarin

Conditions
ConditionsYield
With E. coli whole cells harboring coumarin C-glucosyltransferase from Morus alba (MaCGT) at 30℃; for 24h; Enzymatic reaction;98%
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

D-glucose
50-99-7

D-glucose

2,3,4,5,6-pentakis-O-(trimethylsilyl)-D-glucose
6736-97-6

2,3,4,5,6-pentakis-O-(trimethylsilyl)-D-glucose

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 0 - 20℃;97%
D-glucose
50-99-7

D-glucose

5-amino-1-(6-phenyl-pyridazin-3-yl)-1H-pyrazole-4-carboxylic acid hydrazide
1649475-06-8

5-amino-1-(6-phenyl-pyridazin-3-yl)-1H-pyrazole-4-carboxylic acid hydrazide

5-amino-1-(6-phenyl-pyridazin-3-yl)-1H-pyrazole-4-carboxylic acid (2,3,4,5,6-pentahydroxy-hexylidine)hydrazide

5-amino-1-(6-phenyl-pyridazin-3-yl)-1H-pyrazole-4-carboxylic acid (2,3,4,5,6-pentahydroxy-hexylidine)hydrazide

Conditions
ConditionsYield
With acetic acid In N,N-dimethyl-formamide at 80℃; for 1h;96.93%
D-glucose
50-99-7

D-glucose

acetyl chloride
75-36-5

acetyl chloride

α-D-glucopyranose peracetylate
604-68-2

α-D-glucopyranose peracetylate

Conditions
ConditionsYield
With triethylamine In chloroform at 0 - 10℃; for 2h; Concentration;96.8%
With pyridine; chloroform
D-glucose
50-99-7

D-glucose

5-hydroxymethyl-2-furfuraldehyde
67-47-0

5-hydroxymethyl-2-furfuraldehyde

Conditions
ConditionsYield
With sodium chloride In water at 180℃; for 8h; Catalytic behavior; Reagent/catalyst; Solvent;96%
With chromium chloride; 1-butyl-3-methylimidazolium chloride In toluene at 100℃; for 4h;91%
With aluminium(III) triflate; methanesulfonic acid In dimethyl sulfoxide at 120℃; for 6h; Reagent/catalyst;90%

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