AKOS BBS-00007306

Base Information

• Chemical Name: AKOS BBS-00007306
• CAS No.: 57397-97-4
• Molecular Formula: C10H11NO2
• Molecular Weight: 177.2
• Hs Code.: 2922499990
• Mol file: 57397-97-4.mol

Synonyms:AKOS BBS-00007306;CHEMBRDG-BB 5772307;2-(ALLYLAMINO)BENZOIC ACID;UKRORGSYN-BB BBV-182210;2-(allylamino)benzoic acid(SALTDATA: FREE)

Chemical Property of AKOS BBS-00007306

Chemical Property:

• Vapor Pressure: 4.41E-05mmHg at 25°C
• Boiling Point: 336.4°C at 760 mmHg
• Flash Point: 157.3°C
• PSA: 49.33000
• Density: 1.185g/cm³
• LogP: 2.05570

Purity/Quality:

98% ^*data from raw suppliers

2-(allylamino)benzoicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AKOS BBS-00007306

There total 10 articles about AKOS BBS-00007306 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

anthranilic acid (118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4) + allyl alcohol (107-18-6) → 2-(N-allylamino)benzoic acid (57397-97-4)

Guidance literature:

With palladium diacetate; sodium 3-(diphenylphosphanyl)benzenesulfonate; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1021/jo201691e

Reference yield: 85.0%

2-Iodobenzoic acid (88-67-5) + allylammonium chloride (10017-11-5,110507-15-8,71550-12-4) → 2-(N-allylamino)benzoic acid (57397-97-4)

Guidance literature:

With potassium phosphate; copper(l) iodide; 1,1'-bi-2-naphthol; In N,N-dimethyl-formamide; at 25 ℃; for 16h; Inert atmosphere;

DOI:10.1002/adsc.200900065

Reference yield: 80.0%

allylammonium chloride (10017-11-5,110507-15-8,71550-12-4) + 2-bromobenzoic-acid (88-65-3) → 2-(N-allylamino)benzoic acid (57397-97-4)

Guidance literature:

With potassium phosphate; copper(l) iodide; 1,1'-bi-2-naphthol; In N,N-dimethyl-formamide; at 25 ℃; for 16h; Inert atmosphere;

DOI:10.1002/adsc.200900065

upstream raw materials:

1-allyl-1H-benzo[d][1,3]oxazine-2,4-dione

3-methylsulfanyl-1,3-dihydroindol-2-one

2-azidobenzoic acid

allyl bromide

Downstream raw materials:

1-Allyl-(1H)-chinazolinon-(4)