1,4-Dichloro-2-(2-phenylethenyl)benzene

Base Information

Chemical Name:1,4-Dichloro-2-(2-phenylethenyl)benzene
CAS No.:59425-77-3
Molecular Formula:C₁₄H₁₀Cl₂
Molecular Weight:249.139
Hs Code.:
DSSTox Substance ID:DTXSID10702841
Mol file:59425-77-3.mol

Synonyms:DTXSID10702841;59425-77-3;1,4-dichloro-2-(2-phenylethenyl)benzene

Suppliers and Price of 1,4-Dichloro-2-(2-phenylethenyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,4-Dichloro-2-(2-phenylethenyl)benzene

Chemical Property:

PSA：0.00000
LogP:5.16380
XLogP3:5.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:248.0159557
Heavy Atom Count:16
Complexity:231

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=CC2=C(C=CC(=C2)Cl)Cl

Technology Process of 1,4-Dichloro-2-(2-phenylethenyl)benzene

There total 6 articles about 1,4-Dichloro-2-(2-phenylethenyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 6775-66-2
2,5-dichlorobenzenesulfonylhydrazide

: 59425-77-3
C₁₄H₁₀Cl₂

: 76089-71-9,59425-77-3
2,5-dichloro-stilbene

Guidance literature:: With oxygen; palladium diacetate; In nitromethane; dimethyl sulfoxide; at 70 ℃; for 5h; under 760.051 Torr; optical yield given as %de; stereoselective reaction;
DOI:10.1002/chem.201103671

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 6775-66-2
2,5-dichlorobenzenesulfonylhydrazide

: 59425-77-3
C₁₄H₁₀Cl₂

: 76089-71-9,59425-77-3
2,5-dichloro-stilbene

Guidance literature:: With oxygen; palladium diacetate; In nitromethane; dimethyl sulfoxide; at 70 ℃; for 5h; under 760.051 Torr; optical yield given as %de; stereoselective reaction;
DOI:10.1002/chem.201103671

Reference yield:

: 5402-73-3
2,5-dichlorobenzenesulphonyl chloride

: 59425-77-3
C₁₄H₁₀Cl₂

: 76089-71-9,59425-77-3
2,5-dichloro-stilbene

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2: oxygen; palladium diacetate / nitromethane; dimethyl sulfoxide / 5 h / 70 °C / 760.05 Torr

With oxygen; palladium diacetate; hydrazine hydrate; In tetrahydrofuran; nitromethane; dimethyl sulfoxide; 2: Mizoroki-Heck reaction;
DOI:10.1002/chem.201103671