3-Bromo-5-chloro-4-methoxybenzaldehyde

Base Information

Chemical Name:3-Bromo-5-chloro-4-methoxybenzaldehyde
CAS No.:161565-36-2
Molecular Formula:C8H6BrClO2
Molecular Weight:249.49
Hs Code.:2913000090
DSSTox Substance ID:DTXSID00397503
Nikkaji Number:J632.359F
Wikidata:Q77280720
Metabolomics Workbench ID:115294
Mol file:161565-36-2.mol

Synonyms:3-bromo-5-chloro-4-methoxybenzaldehyde;161565-36-2;DTXSID00397503;CHEMBRDG-BB 6438021;MFCD02629407;STL388900;AKOS002341019;WS-02484;CS-0196358;D86552

Suppliers and Price of 3-Bromo-5-chloro-4-methoxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Bromo-5-chloro-4-methoxybenzaldehyde
500mg
$ 110.00

TRC
3-Bromo-5-chloro-4-methoxybenzaldehyde
100mg
$ 60.00

ChemBridge Corporation
3-bromo-5-chloro-4-methoxybenzaldehyde 95%
250 mg
$ 31.00

AOBChem
3-Bromo-5-chloro-4-methoxybenzaldehyde 95%
10g
$ 296.00

American Custom Chemicals Corporation
3-BROMO-5-CHLORO-4-METHOXYBENZALDEHYDE 95.00%
5G
$ 1018.71

American Custom Chemicals Corporation
3-BROMO-5-CHLORO-4-METHOXYBENZALDEHYDE 95.00%
1G
$ 685.21

Total 7 raw suppliers

Chemical Property of 3-Bromo-5-chloro-4-methoxybenzaldehyde

Chemical Property:

Vapor Pressure:0.000491mmHg at 25°C
Boiling Point:313.6°C at 760 mmHg
Flash Point:143.5°C
PSA：26.30000
Density:1.628g/cm³
LogP:2.92360
Storage Temp.:2-8°C
XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:247.92397
Heavy Atom Count:12
Complexity:165

Purity/Quality:

98% ^*data from raw suppliers

3-Bromo-5-chloro-4-methoxybenzaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1Br)C=O)Cl

Technology Process of 3-Bromo-5-chloro-4-methoxybenzaldehyde

There total 3 articles about 3-Bromo-5-chloro-4-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1849-76-9
3-bromo-5-chloro-4-hydroxybenzaldehyde

: 77-78-1
dimethyl sulfate

: 161565-36-2
3-bromo-5-chloro-4-methoxybenzaldehyde

Guidance literature:: With sodium hydroxide; at 100 ℃; for 0.166667h;
DOI:10.1055/s-2002-35629

Reference yield:

: 2420-16-8
4-hydroxy-3-chlorobenzaldehyde

: 161565-36-2
3-bromo-5-chloro-4-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / Br₂ / acetic acid / 24 h / 80 °C

2: 80 percent / NaOH / 0.17 h / 100 °C

With sodium hydroxide; bromine; In acetic acid;
DOI:10.1055/s-2002-35629

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 161565-36-2
3-bromo-5-chloro-4-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: NCS / CHCl₃ / 1 h / 60 °C

1.2: 76 percent / aq. HCl / CHCl₃ / 12 h / 60 °C

2.1: 60 percent / Br₂ / acetic acid / 24 h / 80 °C

3.1: 80 percent / NaOH / 0.17 h / 100 °C

With sodium hydroxide; N-chloro-succinimide; bromine; In chloroform; acetic acid;
DOI:10.1055/s-2002-35629