3-Bromo-5-chloro-4-hydroxybenzaldehyde

Base Information

Chemical Name:3-Bromo-5-chloro-4-hydroxybenzaldehyde
CAS No.:1849-76-9
Molecular Formula:C7H4BrClO2
Molecular Weight:235.465
Hs Code.:2913000090
European Community (EC) Number:683-352-3
DSSTox Substance ID:DTXSID40395583
Nikkaji Number:J3.163.070C
Wikidata:Q82195740
Mol file:1849-76-9.mol

Synonyms:3-bromo-5-chloro-4-hydroxybenzaldehyde;1849-76-9;SCHEMBL20607030;DTXSID40395583;AKOS B028976;BAA84976;MFCD04129026;STK397883;AKOS000313283;NCGC00340553-01;DS-14801;CS-0059280;3-Bromo-5-chloro-4-hydroxybenzaldehyde, 97%;D73187;AB01333739-02;EN300-7418405;A880747

Suppliers and Price of 3-Bromo-5-chloro-4-hydroxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Bromo-5-chloro-4-hydroxybenzaldehyde
10mg
$ 45.00

Sigma-Aldrich
3-Bromo-5-chloro-4-hydroxybenzaldehyde 97%
1g
$ 50.80

Crysdot
3-Bromo-5-chloro-4-hydroxybenzaldehyde 98%
25g
$ 371.00

CHESS?
MC006907:3-Bromo-5-chloro-4-hydroxy-benzaldehyde 97
5 g
$ 1020.00

CHESS?
MC006907:3-Bromo-5-chloro-4-hydroxy-benzaldehyde 97
1 g
$ 336.00

Chemenu
3-Bromo-5-chloro-4-hydroxybenzaldehyde 95+%
10g
$ 192.00

Chemenu
3-Bromo-5-chloro-4-hydroxybenzaldehyde 95+%
25g
$ 351.00

Chemenu
3-Bromo-5-chloro-4-hydroxybenzaldehyde 95+%
5g
$ 115.00

ChemBridge Corporation
3-bromo-5-chloro-4-hydroxybenzaldehyde 95%
250 mg
$ 31.00

BLDpharm
3-Bromo-5-chloro-4-hydroxybenzaldehyde 97%
5g
$ 109.00

Total 16 raw suppliers

Chemical Property of 3-Bromo-5-chloro-4-hydroxybenzaldehyde

Chemical Property:

Vapor Pressure:0.00584mmHg at 25°C
Melting Point:157-162°C
Boiling Point:264.7°C at 760 mmHg
PKA:4.78±0.23(Predicted)
Flash Point:113.9°C
PSA：37.30000
Density:1.844g/cm³
LogP:2.62060
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:233.90832
Heavy Atom Count:11
Complexity:153

Purity/Quality:

99%, ^*data from raw suppliers

3-Bromo-5-chloro-4-hydroxybenzaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:T
Statements: 25
Safety Statements: 45

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C(=C1Cl)O)Br)C=O

Technology Process of 3-Bromo-5-chloro-4-hydroxybenzaldehyde

There total 4 articles about 3-Bromo-5-chloro-4-hydroxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 2420-16-8
4-hydroxy-3-chlorobenzaldehyde

: 1849-76-9
3-bromo-5-chloro-4-hydroxybenzaldehyde

Guidance literature:: With bromine; In acetic acid; at 80 ℃; for 24h;
DOI:10.1055/s-2002-35629

Reference yield: 26.0%

: 67-56-1
methanol

: 57018-10-7
2-bromo-6-chloro-4-methylphenol

: 1849-76-9
3-bromo-5-chloro-4-hydroxybenzaldehyde

: 2-bromo-6-chloro-4-methoxymethyl-phenol

: 227766-67-8
2-(2-bromo-6-chloro-4-methyl-phenoxy)-6-chloro-4-methoxy-4-methyl-cyclohexa-2,5-dienone

: 2-(2-bromo-6-chloro-4-methoxymethyl-phenoxy)-6-chloro-4-methoxy-4-methyl-cyclohexa-2,5-dienone

Guidance literature:: With perchloric acid; Product distribution; Mechanism; electrolysis at 0.13 mA/cm², 1.4 F/mol, C.C.E. 919 --> 1101 mV vs SCE; electrolyte LiClO4;
DOI:10.1016/S0040-4020(99)00217-3

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1849-76-9
3-bromo-5-chloro-4-hydroxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: NCS / CHCl₃ / 1 h / 60 °C

1.2: 76 percent / aq. HCl / CHCl₃ / 12 h / 60 °C

2.1: 60 percent / Br₂ / acetic acid / 24 h / 80 °C

With N-chloro-succinimide; bromine; In chloroform; acetic acid;
DOI:10.1055/s-2002-35629