5-Methoxy-1H-pyrrolo[2,3-c]pyridine-3-carbaldehyde

Base Information

Chemical Name:5-Methoxy-1H-pyrrolo[2,3-c]pyridine-3-carbaldehyde
CAS No.:227180-23-6
Molecular Formula:C₉H₈N₂O₂
Molecular Weight:176.175
Hs Code.:
Mol file:227180-23-6.mol

Synonyms:5-Methoxy-1H-pyrrolo[2,3-c]pyridine-3-carbaldehyde;5-Methoxy-1H-pyrrolo[2,3-c]pyridine-3-carboxaldehyde;1H-Pyrrolo[2,3-c]pyridine-3-carbaldehyde, 5-Methoxy-

Suppliers and Price of 5-Methoxy-1H-pyrrolo[2,3-c]pyridine-3-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
5-methoxy-1H-pyrrolo[2,3-c]pyridine-3-carbaldehyde 95
10g
$ 4725.00

Chemcia Scientific
5-Methoxy-1H-pyrrolo[2,3-c]pyridine-3-carbaldehyde 95%
5 G
$ 1295.00

American Custom Chemicals Corporation
5-METHOXY-1H-PYRROLO[2,3-C]PYRIDINE-3-CARBALDEHYDE 95.00%
10G
$ 1334.03

American Custom Chemicals Corporation
5-METHOXY-1H-PYRROLO[2,3-C]PYRIDINE-3-CARBALDEHYDE 95.00%
5G
$ 909.56

Total 4 raw suppliers

Chemical Property of 5-Methoxy-1H-pyrrolo[2,3-c]pyridine-3-carbaldehyde

Chemical Property:

Vapor Pressure:4.46E-06mmHg at 25°C
Boiling Point:383.2°C at 760 mmHg
Flash Point:185.6°C
PSA：54.98000
Density:1.347
LogP:1.38400

Purity/Quality:

97% ^*data from raw suppliers

5-methoxy-1H-pyrrolo[2,3-c]pyridine-3-carbaldehyde 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Methoxy-1H-pyrrolo[2,3-c]pyridine-3-carbaldehyde

There total 9 articles about 5-Methoxy-1H-pyrrolo[2,3-c]pyridine-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 17288-53-8
5-Methoxy-1H-pyrrolo[2,3-c]pyridine

: 64-19-7,77671-22-8
acetic acid

: 227180-23-6
3-formyl-5-methoxy-1H-pyrrolo<2,3-c>pyridine

Guidance literature:: With hexamethylenetetramine; at 100 ℃; for 4h;

Reference yield: 38.0%

: 17288-53-8
5-Methoxy-1H-pyrrolo[2,3-c]pyridine

: 100-97-0
hexamethylenetetramine

: 227180-23-6
3-formyl-5-methoxy-1H-pyrrolo<2,3-c>pyridine

Guidance literature:: With acetic acid; In water; for 4h; Heating;
DOI:10.3987/com-98-s(h)111

Reference yield:

: 6628-77-9
6-methoxy-pyridin-3-ylamine

: 227180-23-6
3-formyl-5-methoxy-1H-pyrrolo<2,3-c>pyridine

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 0 deg C, 10 min; RT, 2h

2: 54 percent / t-BuLi, iodine / pentane; tetrahydrofuran / -78 deg C, 75 min; RT, 30 min

3: 66 percent / 10 percent H₂SO₄ / 15 h / Heating

4: 99 percent / Et₃N, CuI / bis(triphenylphosphine)palladium(II) chloride / tetrahydrofuran / 5 h / Ambient temperature

5: 51 percent / CuI / dimethylformamide / 2 h / Heating

6: 38 percent / 33 percent acetic acid / H₂O / 4 h / Heating

With copper(l) iodide; sulfuric acid; iodine; tert.-butyl lithium; acetic acid; triethylamine; bis(triphenylphosphine)palladium(II)-chloride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; pentane;
DOI:10.3987/com-98-s(h)111