2-Bromo-3,4-dimethyl-1-nitrobenzene

Base Information

Chemical Name:2-Bromo-3,4-dimethyl-1-nitrobenzene
CAS No.:101421-62-9
Molecular Formula:C8H8BrNO2
Molecular Weight:230.061
Hs Code.:2904909090
DSSTox Substance ID:DTXSID201293161
Mol file:101421-62-9.mol

Synonyms:2-bromo-3,4-dimethyl-1-nitrobenzene;101421-62-9;3-bromo-1,2-dimethyl-4-nitrobenzene;SCHEMBL3737638;2-bromo-3,4-dimethylnitrobenzene;DTXSID201293161;1-Bromo-2,3-dimethyl-6-nitrobenzene;2-Bromo-3,4-dimethyl-1-nitro-benzene;CS-0339935;FT-0727123;A902901

Suppliers and Price of 2-Bromo-3,4-dimethyl-1-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

J&W Pharmlab
2-Bromo-3,4-dimethyl-1-nitro-benzene 96%
5g
$ 1800.00

J&W Pharmlab
2-Bromo-3,4-dimethyl-1-nitro-benzene 96%
500mg
$ 275.00

J&W Pharmlab
2-Bromo-3,4-dimethyl-1-nitro-benzene 96%
1g
$ 450.00

Crysdot
2-Bromo-3,4-dimethyl-1-nitrobenzene 95+%
1g
$ 429.00

Alichem
1-Bromo-2,3-dimethyl-6-nitrobenzene
1g
$ 1534.70

Alichem
1-Bromo-2,3-dimethyl-6-nitrobenzene
500mg
$ 823.15

Alichem
1-Bromo-2,3-dimethyl-6-nitrobenzene
250mg
$ 470.40

Total 5 raw suppliers

Chemical Property of 2-Bromo-3,4-dimethyl-1-nitrobenzene

Chemical Property:

PSA：45.82000
LogP:3.49730
Storage Temp.:2-8°C
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:228.97384
Heavy Atom Count:12
Complexity:180

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-3,4-dimethyl-1-nitro-benzene 96% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=C(C=C1)[N+](=O)[O-])Br)C

Technology Process of 2-Bromo-3,4-dimethyl-1-nitrobenzene

There total 1 articles about 2-Bromo-3,4-dimethyl-1-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 59146-96-2
2,3-dimethyl-6-nitroaniline

: 101421-62-9
2-bromo-3,4-dimethyl-1-nitrobenzene

Guidance literature:: 2,3-dimethyl-6-nitroaniline; With tert.-butylnitrite; In acetonitrile; at 0 ℃; for 1h;

With copper(ll) bromide; In acetonitrile; at 0 - 25 ℃; for 15h;

Reference yield: 81.0%

: 101421-62-9
2-bromo-3,4-dimethyl-1-nitrobenzene

: 1799434-68-6
2-bromo-3,4-dimethylaniline

Guidance literature:: With water; iron; ammonium chloride; In ethanol; at 80 ℃; for 3.5h; Inert atmosphere;

Reference yield:

: 101421-62-9
2-bromo-3,4-dimethyl-1-nitrobenzene

: tert-butyl 5-acetamido-4-phenylisoindoline-2-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: potassium permanganate / water; pyridine / 4.25 h / 60 - 90 °C

2: urea / o-xylene / 8 h / 150 °C

3: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / 0 - 70 °C

4: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C

5: potassium carbonate / tetrahydrofuran / 0 - 20 °C

6: palladium bis[bis(diphenylphosphino)ferrocene] dichloride; sodium carbonate / 1,4-dioxane; water / 4 h / 80 °C

With sodium tetrahydroborate; potassium permanganate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; boron trifluoride diethyl etherate; sodium carbonate; potassium carbonate; triethylamine; urea; In tetrahydrofuran; 1,4-dioxane; pyridine; o-xylene; water;