2-bromo-3,4-dimethylaniline

Base Information

Chemical Name:2-bromo-3,4-dimethylaniline
CAS No.:1799434-68-6
Molecular Formula:C₈H₁₀BrN
Molecular Weight:200.078
Hs Code.:

Synonyms:

Suppliers and Price of 2-bromo-3,4-dimethylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

J&W Pharmlab
2-Bromo-3,4-dimethylaniline 96%
500mg
$ 449.00

Total 2 raw suppliers

Chemical Property of 2-bromo-3,4-dimethylaniline

Chemical Property:

Boiling Point:267.6±35.0 °C(Predicted)
Density:1.424±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-3,4-dimethylaniline 96% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-bromo-3,4-dimethylaniline

There total 3 articles about 2-bromo-3,4-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 101421-62-9
2-bromo-3,4-dimethyl-1-nitrobenzene

: 1799434-68-6
2-bromo-3,4-dimethylaniline

Guidance literature:: With water; iron; ammonium chloride; In ethanol; at 80 ℃; for 3.5h; Inert atmosphere;

Reference yield:

: 38899-22-8
1,2-dimethyl-4-nitrosobenzene

: 1799434-68-6
2-bromo-3,4-dimethylaniline

: 22364-29-0
2-bromo-4,5-dimethylaniline

Guidance literature:: 1,2-dimethyl-4-nitrosobenzene; With 2,6-di-tert-butyl-4-methyl-phenol; copper(ll) bromide; In acetonitrile; at 20 ℃; for 2h; under 760.051 Torr;

With sodium tetrahydroborate; In acetonitrile; at 20 ℃; for 1h; under 760.051 Torr; Overall yield = 39 %; Overall yield = 23.3 mg; regioselective reaction;
DOI:10.1021/acs.orglett.5b03198

Reference yield:

: 59146-96-2
2,3-dimethyl-6-nitroaniline

: 1799434-68-6
2-bromo-3,4-dimethylaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butylnitrite / acetonitrile / 1 h / 0 °C

1.2: 15 h / 0 - 25 °C

2.1: iron; ammonium chloride; water / ethanol / 3.5 h / 80 °C / Inert atmosphere

With tert.-butylnitrite; water; iron; ammonium chloride; In ethanol; acetonitrile;