phenyl 3-fluoro-6-methoxy-2-methylbenzoate

Base Information

Chemical Name:phenyl 3-fluoro-6-methoxy-2-methylbenzoate
CAS No.:1207283-54-2
Molecular Formula:C15H13FO3
Molecular Weight:260.265
Hs Code.:

Synonyms:phenyl 3-fluoro-6-methoxy-2-methylbenzoate

Suppliers and Price of phenyl 3-fluoro-6-methoxy-2-methylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of phenyl 3-fluoro-6-methoxy-2-methylbenzoate

Chemical Property:

PSA：35.53000
LogP:3.36190

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of phenyl 3-fluoro-6-methoxy-2-methylbenzoate

There total 4 articles about phenyl 3-fluoro-6-methoxy-2-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 220901-72-4
3-fluoro-6-methoxy-2-methylbenzoic acid

: 108-95-2,27073-41-2
phenol

: 1207283-54-2
phenyl 3-fluoro-6-methoxy-2-methylbenzoate

Guidance literature:: 3-fluoro-6-methoxy-2-methylbenzoic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 25 ℃; for 1h;

phenol; With dmap; triethylamine; In dichloromethane; at 25 ℃; for 12h;

Reference yield:

: 394-04-7
5-fluoro-2-methoxybenzoic acid

: 1207283-54-2
phenyl 3-fluoro-6-methoxy-2-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 2 h / -78 °C

1.2: 2 h / -78 - 25 °C

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

2.2: 12 h / 25 °C

With oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;