3-(BENZYLOXY)AZETIDINE BENZENESULFONATE

Base Information

• Chemical Name: 3-(BENZYLOXY)AZETIDINE BENZENESULFONATE
• CAS No.: 897019-59-9
• Molecular Formula: C16H19NO4S
• Molecular Weight: 199.68
• Hs Code.: 2933990090
• Mol file: 897019-59-9.mol

Synonyms:3-(BENZYLOXY)AZETIDINE BENZENESULFONATE;3-(PhenylMethoxy)-azetidine HCl;3-(Benzyloxy)azetidine, HCl;3-(Phenylmethoxy)-azetidinehydrochloride

Chemical Property of 3-(BENZYLOXY)AZETIDINE BENZENESULFONATE

Chemical Property:

• PSA: 21.26000
• LogP: 2.30580
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

3-(Benzyloxy)azetidinebenzenesulfonicacidsalt ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(BENZYLOXY)AZETIDINE BENZENESULFONATE

There total 4 articles about 3-(BENZYLOXY)AZETIDINE BENZENESULFONATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.5%

3-(benzyloxy)azetidine-1-carboxylic acid tert-butyl ester (1027995-71-6) → 3-(benzyloxy)azetidine hydrochloride (897019-59-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

Reference yield: 92.0%

3-(benzyloxy)-1-(diphenylmethyl)azetidine → 3-(benzyloxy)azetidine hydrochloride (897019-59-9)

Guidance literature:

3-(benzyloxy)-1-(diphenylmethyl)azetidine; With carbonochloridic acid 1-chloro-ethyl ester; In 1,2-dichloro-ethane; at 70 ℃; for 1.5h;

With methanol; In 1,2-dichloro-ethane; at 20 - 70 ℃;

Reference yield:

benzyl bromide (100-39-0) → 3-(benzyloxy)azetidine hydrochloride (897019-59-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C

2.1: hydrogenchloride; methanol / 1 h / 20 °C

With hydrogenchloride; methanol; sodium hydride; In N,N-dimethyl-formamide;

upstream raw materials:

benzyl bromide

3-(benzyloxy)azetidine-1-carboxylic acid tert-butyl ester

Downstream raw materials:

N-(4-(3-(benzyloxy)azetidine-1-carbonyl)phenyl)quinoline-8-sulfonamide

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