BAY-1143572.

Base Information

• Chemical Name: BAY-1143572.
• CAS No.: 1414943-88-6
• Molecular Formula: C₁₈H₁₈FN₅O₂S
• Molecular Weight: 387.438
• Mol file: 1414943-88-6.mol

Synonyms:BAY 1143572;BAY1143572;BAY-1143572.

Chemical Property of BAY-1143572.

Chemical Property:

• Boiling Point: 589.9±60.0 °C(Predicted)
• PSA: 109.23000
• Density: 1.36±0.1 g/cm3(Predicted)
• LogP: 4.64490

Purity/Quality:

99%, ^*data from raw suppliers

BAY-1143572 >98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Technology Process of BAY-1143572.

There total 13 articles about BAY-1143572. which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-(4-fluoro-2-methoxyphenyl)-N-{3-[(methylsulfanyl)methyl]phenyl}-1,3,5-triazin-2-amine (1415249-81-8) → (rac)-4-(4-fluoro-2-methoxyphenyl)-N-{3-[(S-methylsulfonimidoyl)methyl]phenyl}-1,3,5-triazin-2-amine (1414943-88-6,1414943-91-1,1414943-94-4)

Guidance literature:

With diacetoxyiodo-3,4,5-trifluorobenzene; water; ammonium carbonate; at 25 ℃; for 16h; Green chemistry;

DOI:10.1002/cssc.201903430

Reference yield: 90.0%

(rac)-ethyl [(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)oxido-λ6-sulfanylidene]carbamate (1414943-84-2) → (rac)-4-(4-fluoro-2-methoxyphenyl)-N-{3-[(S-methylsulfonimidoyl)methyl]phenyl}-1,3,5-triazin-2-amine (1414943-88-6,1414943-91-1,1414943-94-4)

Guidance literature:

With sodium ethanolate; In ethanol; at 60 ℃; for 7h; Inert atmosphere;

DOI:10.1002/cmdc.201700447

Reference yield:

4-(4-fluoro-2-methoxyphenyl)-N-{3-[(S-methylsulfinyl)methyl]phenyl}-1,3,5-triazin-2-amine (1415250-23-5) → (rac)-4-(4-fluoro-2-methoxyphenyl)-N-{3-[(S-methylsulfonimidoyl)methyl]phenyl}-1,3,5-triazin-2-amine (1414943-88-6,1414943-91-1,1414943-94-4)

Guidance literature:

4-(4-fluoro-2-methoxyphenyl)-N-{3-[(S-methylsulfinyl)methyl]phenyl}-1,3,5-triazin-2-amine; With sodium azide; sulfuric acid; In chloroform; at 0 - 45 ℃; for 18h;

With sodium hydrogencarbonate; In tetrahydrofuran; water;

upstream raw materials:

1-[(methylsulfanyl)methyl]-3-nitrobenzene

3-Nitrobenzyl chloride

(rac)-ethyl [(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)oxido-λ⁶-sulfanylidene]carbamate

(rac)-2,2,2-trifluoro-N-[methyl(3-nitrobenzyl)oxido-λ⁶-sulfanylidene]acetamide

Downstream raw materials:

(rac)-N-{3-[(N,S-dimethylsulfonimidoyl)methyl]phenyl}-4-(4-fluoro-2-methoxyphenyl)-l,3,5-triazin-2-amine

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