(2-Chloroethyl)diMethylsulfoniuM iodide

Base Information

• Chemical Name: (2-Chloroethyl)diMethylsulfoniuM iodide
• CAS No.: 25059-70-5
• Molecular Formula: C4H10ClIS
• Molecular Weight: 252.54467
• Hs Code.: 2930909090
• Mol file: 25059-70-5.mol

Synonyms:(2-Chloroethyl)diMethylsulfoniuM iodide

Chemical Property of (2-Chloroethyl)diMethylsulfoniuM iodide

Chemical Property:

• Melting Point: 90-91 °C
• PSA: 25.30000
• LogP: -1.89290

Purity/Quality:

(2-Chloroethyl)dimethylsulfoniumiodide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2-Chloroethyl)diMethylsulfoniuM iodide

There total 3 articles about (2-Chloroethyl)diMethylsulfoniuM iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

sulfure de methyle et de 2-chloroethyle (542-81-4) + methyl iodide (74-88-4) → 2-chloroethyl dimethyl sulfonium iodide (25059-70-5)

Guidance literature:

In methanol; for 18h; Ambient temperature;

DOI:10.1055/s-1999-3444

Reference yield:

sulfure de methyle et de 2-chloroethyle (542-81-4) → 2-chloroethyl dimethyl sulfonium iodide (25059-70-5)

Guidance literature:

In methyl iodide;

Reference yield:

2-chloroethyl sulfide + methyl iodide (74-88-4) → 2-chloroethyl dimethyl sulfonium iodide (25059-70-5)

Guidance literature:

DOI:10.1016/S0040-4039(01)81610-5

upstream raw materials:

sulfure de methyle et de 2-chloroethyle

methyl iodide

Downstream raw materials:

Spiro<2.7>decan-4-one

spiro[2.5]octan-4-one

2,4-dichlorophenyl 1-(pyridin-3-yl)-cyclopropyl ketone

tert-butyl 8-oxo-5-azaspiro[2.5]octane-5-carboxylate

Refernces

• 1、 -. "ALDOSTERONE SYNTHASE INHIBITORS". Page/Page column 48-49. . Retrieved 2016/06/28.
• 2、 Kraft, Philip. "Design and synthesis of violet odorants with bicyclo[6.4.0]dodecene and bicyclo[5.4.0]undecene skeletons". . p. 695 - 703. Retrieved 2007/10/03.