5-Chloro-2-propoxypyridine

Base Information

• Chemical Name: 5-Chloro-2-propoxypyridine
• CAS No.: 1160018-61-0
• Molecular Formula: C8H10ClNO
• Molecular Weight: 171.62
• Hs Code.: 2933399990
• Mol file: 1160018-61-0.mol

Synonyms:5-Chloro-2-propoxypyridine

Chemical Property of 5-Chloro-2-propoxypyridine

Chemical Property:

• Boiling Point: 215.0±20.0 °C(Predicted)
• PKA: 1.83±0.22(Predicted)
• PSA: 22.12000
• Density: 1.131±0.06 g/cm3(Predicted)
• LogP: 2.52380

Purity/Quality:

99% ^*data from raw suppliers

5-Chloro-2-propoxypyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Chloro-2-propoxypyridine

There total 1 articles about 5-Chloro-2-propoxypyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

propan-1-ol (71-23-8) + 2-fluoro-5-chloropyridine (1480-65-5) → 5-chloro-2-propoxypyridine (1160018-61-0)

Guidance literature:

propan-1-ol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 5 ℃; for 2h; Inert atmosphere;

2-fluoro-5-chloropyridine; In tetrahydrofuran; mineral oil; at 5 - 20 ℃; Product distribution / selectivity;

Reference yield: 74.0%

5-chloro-2-propoxypyridine (1160018-61-0) → 5-chloro-2-propoxy-4-pyridinylboronic acid (1196699-78-1)

Guidance literature:

5-chloro-2-propoxypyridine; With lithium diisopropyl amide; In tetrahydrofuran; at -82 - 78 ℃; for 3h; Inert atmosphere;

With Triisopropyl borate; In tetrahydrofuran; at -82 - 78 ℃; for 3.5h;

With water; In tetrahydrofuran; at -82 - 20 ℃; Product distribution / selectivity;

upstream raw materials:

propan-1-ol

2-fluoro-5-chloropyridine

Downstream raw materials:

5-chloro-2-propoxy-4-pyridinylboronic acid

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