1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-3-methoxy-1-methyl-, 3R-(3.alpha.,3a.alpha.,4.alpha.,5.beta.,6.alpha.,6a.alpha.)-

Base Information

Chemical Name:1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-3-methoxy-1-methyl-, 3R-(3.alpha.,3a.alpha.,4.alpha.,5.beta.,6.alpha.,6a.alpha.)-
CAS No.:88111-92-6
Molecular Formula:C₈H₁₅NO₅
Molecular Weight:205.211
Hs Code.:
Mol file:88111-92-6.mol

Synonyms:1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-3-methoxy-1-methyl-, 3R-(3.alpha.,3a.alpha.,4.alpha.,5.beta.,6.alpha.,6a.alpha.)-

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-3-methoxy-1-methyl-, 3R-(3.alpha.,3a.alpha.,4.alpha.,5.beta.,6.alpha.,6a.alpha.)-

Chemical Property:

PSA：82.39000
LogP:-2.14510

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-3-methoxy-1-methyl-, 3R-(3.alpha.,3a.alpha.,4.alpha.,5.beta.,6.alpha.,6a.alpha.)-

There total 3 articles about 1H-Cyclopentcisoxazole-4,5,6-triol, hexahydro-3-methoxy-1-methyl-, 3R-(3.alpha.,3a.alpha.,4.alpha.,5.beta.,6.alpha.,6a.alpha.)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67-56-1
methanol

: 88111-90-4
(1R,5S)-6-exo,7-endo,8-exo-trihydroxy-N-methyl-4-endo-phenylthio-3-oxa-2-azabicyclo<3.3.0>octane

: 88111-92-6
(1R,5S)-6-exo,7-endo,8-exo-trihydroxy-4-exo-methoxy-N-methyl-3-oxa-2-azabicyclo<3.3.0>octane

Guidance literature:: With mercury(II) diacetate; for 0.0333333h;

Reference yield:

: Acetic acid (E)-(1S,2R)-2-acetoxy-1-((R)-1-acetoxy-2-oxo-ethyl)-4-phenylsulfanyl-but-3-enyl ester

: 88111-92-6
(1R,5S)-6-exo,7-endo,8-exo-trihydroxy-4-exo-methoxy-N-methyl-3-oxa-2-azabicyclo<3.3.0>octane

Guidance literature:: Multi-step reaction with 3 steps

1: 38 percent / pyridine, N-methylhydroxylamine hydrochloride / ethanol / 0.5 h / 50 °C

2: 82 percent / sodium methoxide / methanol

3: 70 percent / mercury⁽¹¹⁾ acetate / 0.03 h

With pyridine; N-methylhydroxyamine hydrochloride; mercury(II) diacetate; sodium methylate; In methanol; ethanol;

Reference yield:

: 88111-83-5
(1R,5S)-6-exo,7-endo,8-exo-triacetoxy-N-methyl-4-endo-phenylthio-3-oxa-2-azabicyclo<3.3.0>octane

: 88111-92-6
(1R,5S)-6-exo,7-endo,8-exo-trihydroxy-4-exo-methoxy-N-methyl-3-oxa-2-azabicyclo<3.3.0>octane

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / sodium methoxide / methanol

2: 70 percent / mercury⁽¹¹⁾ acetate / 0.03 h

With mercury(II) diacetate; sodium methylate; In methanol;