3-Deoxy-galactosone

Base Information

• Chemical Name: 3-Deoxy-galactosone
• CAS No.: 4134-97-8
• Molecular Formula: C₆H₁₀O₅
• Molecular Weight: 162.142
• Hs Code.: 2914409000
• Mol file: 4134-97-8.mol

Synonyms:3-Deoxy-D-threo-hexos-2-ulose;3-Deoxy-D-threo-hexosulose;3-Deoxy-galactosone;3-Deoxy-galactosone (90%)

Chemical Property of 3-Deoxy-galactosone

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 440.724°C at 760 mmHg
• Flash Point: 191.85°C
• PSA: 86.99000
• Density: 1.522g/cm³
• LogP: -1.98400
• Storage Temp.: -86°C Freezer, Under Inert Atmosphere
• Solubility.: Acetonitrile (Slightly), Methanol (Sparingly), Water (Slightly, Sonicated)

Purity/Quality:

98%Min ^*data from raw suppliers

3-Deoxygalactosone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: It has carcinostatic activity. It has carcinostatic activity

Technology Process of 3-Deoxy-galactosone

There total 14 articles about 3-Deoxy-galactosone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-glucose (50-99-7) → furfural (98-01-1) + 5-hydroxymethyl-2-furfuraldehyde (67-47-0) + D-Fructose (57-48-7,18875-34-8) + 2,3-dihydro-3,5-dihydroxy-6-methyl-4H-pyran-4-one (28564-83-2) + D-glucosone (643-71-0,25990-59-4,26187-86-0,26345-59-5,49865-02-3,54142-77-7,81844-97-5,81844-98-6,81845-00-3,89576-70-5,90457-64-0,1854-25-7) + 3-deoxygalactosone (4084-27-9,30382-30-0,50455-94-2,82399-12-0,4134-97-8) + 3-deoxyglucosone (4134-97-8,30382-30-0,50455-94-2,82399-12-0,4084-27-9) + 1-deoxy-2,3-D-erythro-hexo-2,3-diulose + 3-deoxypentos-2-ulose + 1,4-dideoxyhexosulose

Guidance literature:

With L-alanin; In water; at 130 ℃; for 5h; pH=5.0; Time; Sealed tube;

DOI:10.1021/acs.jafc.7b04105

Reference yield:

D-glucose (50-99-7) → furfural (98-01-1) + 5-hydroxymethyl-2-furfuraldehyde (67-47-0) + D-Fructose (57-48-7,18875-34-8) + 2,3-dihydro-3,5-dihydroxy-6-methyl-4H-pyran-4-one (28564-83-2) + D-glucosone (643-71-0,25990-59-4,26187-86-0,26345-59-5,49865-02-3,54142-77-7,81844-97-5,81844-98-6,81845-00-3,89576-70-5,90457-64-0,1854-25-7) + 3-deoxygalactosone (4084-27-9,30382-30-0,50455-94-2,82399-12-0,4134-97-8) + 3-deoxyglucosone (4134-97-8,30382-30-0,50455-94-2,82399-12-0,4084-27-9) + 1-deoxy-2,3-D-erythro-hexo-2,3-diulose + 3-deoxypentos-2-ulose + 1,4-dideoxyhexosulose

Guidance literature:

With L-alanin; In water; at 130 ℃; for 5h; pH=5.0; Time; Sealed tube;

DOI:10.1021/acs.jafc.7b04105

Reference yield:

D-maltose (69-79-4) → furfural (98-01-1) + 1-(2-furyl)-1-ethanone (1192-62-7,80145-44-4) + 5-hydroxymethyl-2-furfuraldehyde (67-47-0) + Maltol (118-71-8) + D-Fructose (57-48-7,18875-34-8) + 2,3-dihydro-3,5-dihydroxy-6-methyl-4H-pyran-4-one (28564-83-2) + D-glucose (50-99-7) + D-glucosone (643-71-0,25990-59-4,26187-86-0,26345-59-5,49865-02-3,54142-77-7,81844-97-5,81844-98-6,81845-00-3,89576-70-5,90457-64-0,1854-25-7) + 3-deoxygalactosone (4084-27-9,30382-30-0,50455-94-2,82399-12-0,4134-97-8) + 3-deoxyglucosone (4134-97-8,30382-30-0,50455-94-2,82399-12-0,4084-27-9) + 1-deoxymaltosone + 3-deoxymaltosone + 3-deoxypentos-2-ulose + 1,4-dideoxyhexosulose

Guidance literature:

With L-alanin; In water; at 130 ℃; for 5h; pH=5.0; Time; Sealed tube;

DOI:10.1021/acs.jafc.7b04105

upstream raw materials:

D-maltose

D-glucose

N-(1-deoxy-D-fructos-1-yl)-L-glycine

L-Lysine hydrochloride

Downstream raw materials:

(3-Desoxy-D-threo-hexosulose)-2,4-dinitrophenyl-osazon

3-Desoxy-D-galactoson-bis-(2,5-dichlor-phenylhydrazon)

D-erythro-3-deoxy-[2]hexosulose-bis-(4-nitro-phenylhydrazone)

D-erythro-3-deoxy-[2]hexosulose-bis-(2,4-dinitro-phenylhydrazone)