4-nitrobenzyl 2-hydroxybenzoate

Base Information

Chemical Name:4-nitrobenzyl 2-hydroxybenzoate
CAS No.:85303-65-7
Molecular Formula:C14H11NO5
Molecular Weight:273.24
Hs Code.:

Synonyms:CHEMBRDG-BB 5235286;4-NITROBENZYL SALICYLATE

Suppliers and Price of 4-nitrobenzyl 2-hydroxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

American Custom Chemicals Corporation
4-NITROBENZYLSALICYLATE 95.00%
5MG
$ 503.62

Total 0 raw suppliers

Chemical Property of 4-nitrobenzyl 2-hydroxybenzoate

Chemical Property:

Vapor Pressure:2.71E-08mmHg at 25°C
Boiling Point:438.3°C at 760 mmHg
Flash Point:218.9°C
PSA：92.35000
Density:1.377g/cm³
LogP:3.18060

Purity/Quality:: 4-NITROBENZYLSALICYLATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 4-nitrobenzyl 2-hydroxybenzoate

There total 4 articles about 4-nitrobenzyl 2-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 619-73-8
4-nitrobenzyl chloride

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 85303-65-7
salicylic acid 4-nitrobenzyl ester

Guidance literature:: salicylic acid; With (E)-ethyl 2-cyano-2-(2-nitrophenylsulfonyloxyimino)acetate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 25 ℃;

4-nitrobenzyl chloride; In dichloromethane; at 25 ℃; for 2h; chemoselective reaction;
DOI:10.1021/jo500292m

Reference yield:

: 54-21-7
sodium salicylate

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 85303-65-7
salicylic acid 4-nitrobenzyl ester

Guidance literature:: With ethanol;

Reference yield:

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 85303-65-7
salicylic acid 4-nitrobenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 4.4 g / dicyclohexylcarbodiimide / acetone / 3 h

2: DMAP / acetonitrile / 1 h / Ambient temperature

With dmap; dicyclohexyl-carbodiimide; In acetone; acetonitrile;
DOI:10.1016/0031-9422(94)00662-D