3a,4,4a,5,8,8a,9,9a-octahydro-4,9:5,8-dimethano-1H-benz[f]indene

Base Information

• Chemical Name: 3a,4,4a,5,8,8a,9,9a-octahydro-4,9:5,8-dimethano-1H-benz[f]indene
• CAS No.: 35184-08-8
• Molecular Formula: C₁₅H₁₈
• Molecular Weight: 198.308
• Mol file: 35184-08-8.mol

Synonyms:3a,4,4a,5,8,8a,9,9a-octahydro-4,9:5,8-dimethano-1H-benz[f]indene;4,9:5,8-Dimethano-1H-benzfindene, 3a,4,4a,5,8,8a,9,9a-octahydro-;[Mixture of 3a,4,4a,5,8,8a,9,9a-Octahydro-4,9:5,8-dimethano-1H-benz[f]indene(7158-25-0) and 4,4a,4b,5,8,8a,9,9a-Octahydro-1,4:5,8-dimethano-1H-fluorene(35184-08-8)]

Chemical Property of 3a,4,4a,5,8,8a,9,9a-octahydro-4,9:5,8-dimethano-1H-benz[f]indene

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3a,4,4a,5,8,8a,9,9a-octahydro-4,9:5,8-dimethano-1H-benz[f]indene

There total 8 articles about 3a,4,4a,5,8,8a,9,9a-octahydro-4,9:5,8-dimethano-1H-benz[f]indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methylfuran (534-22-5) + bi(cyclopentadiene) (77-73-6,933-60-8,1755-01-7,25038-78-2) → pentacyclo[6.5.1.13.6.0 2, 7.0 9,13]pentadecane-4,10-diene (35184-08-8,36806-65-2,64599-31-1,64599-32-2) + endo,exo,endo-pentacyclo<6.5.1.02,7.13,6.09,13>pentadeca-4,10-diene (7158-25-0) + C20H24O + 4-methyl-4,4a,4b,5,8,8a,9,9a-octahydro-1H-1,4-epoxy-5,8-methanofluorene + 8-methyl-3a,4,4a,5,8,8a,9,9a-octahydro-1H-5,8-epoxy-4,9-methanocyclopenta[b]naphthalene + 4-methyl-3a,4,7,7a-tetrahydro-1H-4,7-epoxyindene + C20H24O + C20H24O

Guidance literature:

With acidic zeolite; at 150 ℃; for 5h; under 3750.38 Torr; Reagent/catalyst; Temperature; Autoclave; Inert atmosphere;

DOI:10.1016/j.cattod.2018.04.053

Reference yield:

bi(cyclopentadiene) (77-73-6,933-60-8,1755-01-7,25038-78-2) + cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) → pentacyclo[6.5.1.13.6.0 2, 7.0 9,13]pentadecane-4,10-diene (35184-08-8,36806-65-2,64599-31-1,64599-32-2) + endo,exo,endo-pentacyclo<6.5.1.02,7.13,6.09,13>pentadeca-4,10-diene (7158-25-0)

Guidance literature:

at 155 - 160 ℃; for 10h; under 1500.15 Torr;

Reference yield:

endo-Dicyclopentadien (1755-01-7,25038-78-2) + cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) → (+/-)-(3arH.4atH.8atH.9acH)-3a.4.4a.5.8.8a.9.9a-octahydro-1H-4c.9c:5t.8t-dimethano-cyclopenta[b]naphthalene (7158-25-0,23197-85-5,24809-51-6,24809-52-7,24809-53-8) + C15H18 (35184-08-8,36806-65-2,64599-31-1,64599-32-2) + C15H18 (35184-08-8,36806-65-2,64599-31-1,64599-32-2) + C15H18 (35184-08-8,36806-65-2,64599-31-1,64599-32-2)

Guidance literature:

at 180 ℃; for 2h; Thermodynamic data; Rate constant; activation parameters, ΔH(excit.), ΔS(excit.);

upstream raw materials:

carbon monoxide

bi(cyclopentadiene)

cyclopenta-1,3-diene

2-methylfuran

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