Methyl 4-(5-hydroxy-5-methyl-3-oxoisoxazolidin-2-yl)benzoate

Base Information

• Chemical Name: Methyl 4-(5-hydroxy-5-methyl-3-oxoisoxazolidin-2-yl)benzoate
• CAS No.: 371166-28-8
• Molecular Formula: C12H13NO5
• Molecular Weight: 251.24
• Hs Code.: 2934999090
• Mol file: 371166-28-8.mol

Synonyms:Methyl 4-(5-hydroxy-5-methyl-3-oxoisoxazolidin-2-yl)benzoate

Chemical Property of Methyl 4-(5-hydroxy-5-methyl-3-oxoisoxazolidin-2-yl)benzoate

Chemical Property:

• PSA: 76.07000
• LogP: 0.91500

Purity/Quality:

≥99% ^*data from raw suppliers

Methyl4-(5-hydroxy-5-methyl-3-oxoisoxazolidin-2-yl)benzoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 4-(5-hydroxy-5-methyl-3-oxoisoxazolidin-2-yl)benzoate

There total 1 articles about Methyl 4-(5-hydroxy-5-methyl-3-oxoisoxazolidin-2-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

4-methyleneoxetan-2-one (674-82-8,2130-41-8) + N-[(4-methoxycarbonyl)phenyl]hydroxylamine (24226-29-7) → 5-hydroxy-2-(4-methoxycarbonyl-phenyl)-5-methylisoxazolidin-3-one (371166-28-8)

Guidance literature:

Reference yield: 92.0%

thiobenzoylhydrazine (20605-40-7) + 5-hydroxy-2-(4-methoxycarbonyl-phenyl)-5-methylisoxazolidin-3-one (371166-28-8) → 5-[N-hydroxy-N-(4-methoxycarbonylphenylacetamido)]-5-methyl-2-phenyl-Δ2-1,3,4-thiadiazoline

Guidance literature:

With trifluoroacetic acid;

Reference yield: 90.0%

4-methylthiobenzoylhydrazine (71025-26-8) + 5-hydroxy-2-(4-methoxycarbonyl-phenyl)-5-methylisoxazolidin-3-one (371166-28-8) → 5-[N-hydroxy-N-(4-methoxycarbonylphenylacetamido)]-5-methyl-2-(4-tolyl)-Δ2-1,3,4-thiadiazoline

Guidance literature:

With trifluoroacetic acid;

upstream raw materials:

4-methyleneoxetan-2-one

N-[(4-methoxycarbonyl)phenyl]hydroxylamine

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