3β-(Acetyloxy)-14β-hydroxy-5β-androstane-17β-carboxylic acid methyl ester

Base Information

Chemical Name:3β-(Acetyloxy)-14β-hydroxy-5β-androstane-17β-carboxylic acid methyl ester
CAS No.:2900-98-3
Molecular Formula:C23H36O5
Molecular Weight:392.52894
Hs Code.:
Mol file:2900-98-3.mol

Synonyms:3β-(Acetyloxy)-14β-hydroxy-5β-androstane-17β-carboxylic acid methyl ester

Suppliers and Price of 3β-(Acetyloxy)-14β-hydroxy-5β-androstane-17β-carboxylic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of 3β-(Acetyloxy)-14β-hydroxy-5β-androstane-17β-carboxylic acid methyl ester

Chemical Property:

Melting Point:151 - 154 °C
PSA：72.83000
LogP:3.86490

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 3β-(Acetyloxy)-14β-hydroxy-5β-androstane-17β-carboxylic acid methyl ester

There total 24 articles about 3β-(Acetyloxy)-14β-hydroxy-5β-androstane-17β-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26623-72-3
5β,14β-Pregnan-3β,14,20ξ,21-tetraol

: 2900-98-3
3β-Acetoxy-14-hydroxy-5β,14β-androstan-17β-carbonsaeuremethylester

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / NaIO₄ / methanol / 1.5 h / Ambient temperature

2: pyridine / 15 h / Ambient temperature

3: KMnO₄, Jones reagent / acetone / 0.25 h

4: methanol

With potassium permanganate; sodium periodate; jones reagent; In pyridine; methanol; acetone;

Reference yield:

: 26623-73-4
3β,14β-dihydroxy-5β-androstane-17β-carboxaldehyde

: 2900-98-3
3β-Acetoxy-14-hydroxy-5β,14β-androstan-17β-carbonsaeuremethylester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 15 h / Ambient temperature

2: KMnO₄, Jones reagent / acetone / 0.25 h

3: methanol

With potassium permanganate; jones reagent; In pyridine; methanol; acetone;

Reference yield:

: 53297-44-2
3β-Acetoxy-20-oxo-5β,14β-pregnan-21,14-lacton

: 2900-98-3
3β-Acetoxy-14-hydroxy-5β,14β-androstan-17β-carbonsaeuremethylester

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / LiAlH₄ / tetrahydrofuran / 1 h / Heating

2: 86 percent / NaIO₄ / methanol / 1.5 h / Ambient temperature

3: pyridine / 15 h / Ambient temperature

4: KMnO₄, Jones reagent / acetone / 0.25 h

5: methanol

With potassium permanganate; sodium periodate; lithium aluminium tetrahydride; jones reagent; In tetrahydrofuran; pyridine; methanol; acetone;