N,O-Diacetyl-DL-Serine methyl ester

Base Information

Chemical Name:N,O-Diacetyl-DL-Serine methyl ester
CAS No.:55299-57-5
Molecular Formula:C8H13NO5
Molecular Weight:203.195
Hs Code.:
Mol file:55299-57-5.mol

Synonyms:N,O-Diacetyl-DL-Serine methyl ester

Suppliers and Price of N,O-Diacetyl-DL-Serine methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of N,O-Diacetyl-DL-Serine methyl ester

Chemical Property:

Boiling Point:160 °C(Press: 8 Torr)
PKA:14.10±0.46(Predicted)
PSA：81.70000
Density:1.168±0.06 g/cm3(Predicted)
LogP:-0.38190

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N,O-Diacetyl-DL-Serine methyl ester

There total 4 articles about N,O-Diacetyl-DL-Serine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.7%

: 5619-04-5
methyl 2-amino-3-hydroxypropanoate hydrochloride

: 75-36-5
acetyl chloride

: 55299-57-5
2-acetylamino-3-methoxy-3-oxo-propyl acetate

Guidance literature:: With triethylamine; In ethyl acetate; at 20 ℃; for 2h; Cooling with ice;

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1068-84-4
2-aminomalonic acid

: 108-24-7
acetic anhydride

: 55299-57-5
2-acetylamino-3-methoxy-3-oxo-propyl acetate

: 55299-56-4,2311-26-4,54322-41-7,288402-26-6
N-acetyl serine methyl ester

: 4-carbomethoxy-2-hydroxy-2-methyl-1,3-oxazole

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1080/00397919208021300

Reference yield:

: 108-24-7
acetic anhydride

: 5619-04-5
methyl 2-amino-3-hydroxypropanoate hydrochloride

: 55299-57-5
2-acetylamino-3-methoxy-3-oxo-propyl acetate

Guidance literature:: methyl 2-amino-3-hydroxypropanoate hydrochloride; With triethylamine; In acetonitrile; Large scale reaction;

acetic anhydride; In acetonitrile; at 0 - 20 ℃;
DOI:10.1021/op200065p