N,N'-Bis(2,2-dimethylpropionyl)-o-phenylenediamine

Base Information

Chemical Name:N,N'-Bis(2,2-dimethylpropionyl)-o-phenylenediamine
CAS No.:93142-62-2
Molecular Formula:C₁₆H₂₄N₂O₂
Molecular Weight:276.379
Hs Code.:
DSSTox Substance ID:DTXSID10918662
Nikkaji Number:J156.661J
Wikidata:Q82890877
ChEMBL ID:CHEMBL4900444

Synonyms:BRN 4257089;Propionamide, N,N'-phenylenebis(2,2-dimethyl-;93142-62-2;N,N'-Bis(2,2-dimethylpropionyl)-o-phenylenediamine;N-[2-(2,2-Dimethyl-propionylamino)-phenyl]-2,2-dimethyl-propionamide;Oprea1_609268;SCHEMBL5706504;CHEMBL4900444;DTXSID10918662;HMS1589H13;STK439539;AKOS003300147;SR-01000255354;N,N'-benzene-1,2-diylbis(2,2-dimethylpropanamide);SR-01000255354-1;N,N'-1,2-PHENYLENEBIS(2,2-DIMETHYLPROPANAMIDE);N,N'-(1,2-Phenylene)bis(2,2-dimethylpropanimidic acid)

Suppliers and Price of N,N'-Bis(2,2-dimethylpropionyl)-o-phenylenediamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N,N'-Bis(2,2-dimethylpropionyl)-o-phenylenediamine

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:276.183778013
Heavy Atom Count:20
Complexity:328

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C(=O)NC1=CC=CC=C1NC(=O)C(C)(C)C

Technology Process of N,N'-Bis(2,2-dimethylpropionyl)-o-phenylenediamine

There total 6 articles about N,N'-Bis(2,2-dimethylpropionyl)-o-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3282-30-2
pivaloyl chloride

: 95-54-5
1,2-diamino-benzene

: 93142-62-2
2,2,2',2'-Tetramethyl-N,N'-(phen-1,2-ylen)bis

Guidance literature:: With triethylamine; In dichloromethane; Ambient temperature;
DOI:10.1002/hlca.19930760120

Reference yield: 52.0%

: 6625-74-7
N-pivaloylaniline

: 114379-11-2
3-(tert-butyl)-1,4,2-dioxazol-5-one

: N,N',N''-(benzene-1,2,3-triyl)tris(2,2-dimethylpropanamide)

: 93142-62-2
2,2,2',2'-Tetramethyl-N,N'-(phen-1,2-ylen)bis

Guidance literature:: With silver hexafluoroantimonate; [RhCl₂(p-cymene)]2; In 1,2-dichloro-ethane; at 40 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201701138

Reference yield:

: 62-53-3
aniline

: N,N',N''-(benzene-1,2,3-triyl)tris(2,2-dimethylpropanamide)

: 93142-62-2
2,2,2',2'-Tetramethyl-N,N'-(phen-1,2-ylen)bis

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere

2: [RhCl₂(p-cymene)]2; silver hexafluoroantimonate / 1,2-dichloro-ethane / 12 h / 40 °C / Inert atmosphere

With silver hexafluoroantimonate; [RhCl₂(p-cymene)]2; triethylamine; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1002/anie.201701138