3-BroMo-N,N,5-triMethylbenzenesulfonaMide

Base Information

Chemical Name:3-BroMo-N,N,5-triMethylbenzenesulfonaMide
CAS No.:1020252-92-9
Molecular Formula:C7H5BrF3NO
Molecular Weight:278.17
Hs Code.:2935009090
Mol file:1020252-92-9.mol

Synonyms:Bromides;((4-Bromo-3-methylphenyl)carbonyl)morpholine;(4-Bromo-3-methylphenyl)(morpholino)methanone;(3-Bromobenzoyl)pyrrolidine;(3-Bromophenyl)(pyrrolidin-1-yl)methanone;(4-Bromo-2-fluorophenyl)(4-methoxybenzyl)sulfane;S-(4-Methoxybenzyl) 4-bromo-2-fluorothiophenol;(4-Bromo-3-methylphenyl)(pyrrolidin-1-yl)methanone

Suppliers and Price of 3-BroMo-N,N,5-triMethylbenzenesulfonaMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N,N-Dimethyl3-bromo-5-methylbenzenesulfonamide
1g
$ 165.00

TRC
N,N-Dimethyl3-bromo-5-methylbenzenesulfonamide
100mg
$ 45.00

Crysdot
3-Bromo-N,N,5-trimethylbenzenesulfonamide 95+%
5g
$ 339.00

Crysdot
3-Bromo-N,N,5-trimethylbenzenesulfonamide 95+%
10g
$ 564.00

American Custom Chemicals Corporation
3-BROMO-N,N,5-TRIMETHYLBENZENESULFONAMIDE 95.00%
5MG
$ 503.14

AK Scientific
N,N-Dimethyl3-bromo-5-methylbenzenesulfonamide
5g
$ 531.00

AK Scientific
N,N-Dimethyl3-bromo-5-methylbenzenesulfonamide
1g
$ 211.00

Total 9 raw suppliers

Chemical Property of 3-BroMo-N,N,5-triMethylbenzenesulfonaMide

Chemical Property:

Melting Point:45-46°C
Boiling Point:363.3±52.0 °C(Predicted)
PKA:-4.89±0.70(Predicted)
PSA：45.76000
Density:1.484±0.06 g/cm3(Predicted)
LogP:3.08860
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

N,N-Dimethyl3-bromo-5-methylbenzenesulfonamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-BroMo-N,N,5-triMethylbenzenesulfonaMide

There total 1 articles about 3-BroMo-N,N,5-triMethylbenzenesulfonaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 885520-33-2
3-bromo-5-methylbenzene-1-sulfonyl chloride

: 124-40-3
dimethyl amine

: 1020252-92-9
3-bromo-N,N,5-trimethylbenzenesulfonamide

Guidance literature:: In dichloromethane; at 20 ℃; for 0.333333h; Cooling with ice;

Reference yield: 73.0%

: 1013-88-3
Benzophenone imine

: 1020252-92-9
3-bromo-N,N,5-trimethylbenzenesulfonamide

: 1335140-35-6
3-[(diphenylmethylidene)amino]-N,N,5-trimethylbenzenesulfonamide

Guidance literature:: With caesium carbonate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; at 130 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 1020252-92-9
3-bromo-N,N,5-trimethylbenzenesulfonamide

: 1017475-23-8
3-amino-N,N,5-trimethylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 0.5 h / 130 °C / Inert atmosphere

2: hydrogenchloride; water / tetrahydrofuran / 1 h / 20 °C

With hydrogenchloride; water; caesium carbonate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; 1,4-dioxane;