Ethanol, 2-(2-benzothiazolylmethylamino)- (9CI)

Base Information

• Chemical Name: Ethanol, 2-(2-benzothiazolylmethylamino)- (9CI)
• CAS No.: 68720-62-7
• Molecular Formula: C10H12N2OS
• Molecular Weight: 208.284
• Mol file: 68720-62-7.mol

Synonyms:2-(benzothiazol-2-yl-methyl-amino)-ethanol;2[N-methyl-N-(2-benzothiazolyl)amino]ethanol;2-(benzothiazol-2-yl-methylamino)ethanol;2-[N-methyl-N-(2-benzothiazolyl)amino]ethanol;2-[1,3-benzothiazol-2-yl(methyl)amino]ethanol;

Chemical Property of Ethanol, 2-(2-benzothiazolylmethylamino)- (9CI)

Chemical Property:

• PSA: 64.60000
• LogP: 1.72480

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanol, 2-(2-benzothiazolylmethylamino)- (9CI)

There total 2 articles about Ethanol, 2-(2-benzothiazolylmethylamino)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

(2-hydroxyethyl)(methyl)amine (109-83-1) + 2-chlorobenzo[d][1,3]thiazole (615-20-3) → 2-[N-Methyl-N-(2-benzothiazolyl)amino]ethanol (68720-62-7)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 60 - 70 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.bmcl.2011.03.027

Reference yield:

(2-hydroxyethyl)(methyl)amine (109-83-1) + silica-gel + 2-chlorobenzo[d][1,3]thiazole (615-20-3) → 4-[2-(N-Methyl-N-(2-benzothiazolyl)amino)ethoxy]-benzaldehyde (122320-75-6) + 2-[N-Methyl-N-(2-benzothiazolyl)amino]ethanol (68720-62-7)

Guidance literature:

In methanol; dichloromethane; water;

Reference yield: 74.0%

methyl α-methoxy-(p-hydroxyphenyl)acetate (76529-98-1) + 2-[N-Methyl-N-(2-benzothiazolyl)amino]ethanol (68720-62-7) → methyl 2-(4-{2-[1,3-benzothiazol-2-yl(methyl)amino]ethoxy}phenyl)-2-methoxyacetate

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;

upstream raw materials:

(2-hydroxyethyl)(methyl)amine

2-chlorobenzo[d][1,3]thiazole

Downstream raw materials:

4-[2-(N-Methyl-N-(2-benzothiazolyl)amino)ethoxy]-benzaldehyde

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