N-((6-Methylpyridin-2-YL)methyl)formamide

Base Information

• Chemical Name: N-((6-Methylpyridin-2-YL)methyl)formamide
• CAS No.: 54384-88-2
• Molecular Formula: C₈H₁₀N₂O
• Molecular Weight: 150.18
• Hs Code.: 2933399090
• DSSTox Substance ID: DTXSID20480643
• Wikidata: Q82315584
• Mol file: 54384-88-2.mol

Synonyms:N-((6-METHYLPYRIDIN-2-YL)METHYL)FORMAMIDE;54384-88-2;N-[(6-methylpyridin-2-yl)methyl]formamide;N-(6-Methyl-pyridin-2-ylmethyl)-formamide;DTXSID20480643;AKOS006310555;SB54177

Chemical Property of N-((6-Methylpyridin-2-YL)methyl)formamide

Chemical Property:

• PSA: 45.48000
• LogP: 1.47630
• Storage Temp.: 2-8°C
• XLogP3: 0.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 150.079312947
• Heavy Atom Count: 11
• Complexity: 127

Purity/Quality:

95% ^*data from raw suppliers

N-((6-Methylpyridin-2-yl)methyl)formamide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=NC(=CC=C1)CNC=O

Technology Process of N-((6-Methylpyridin-2-YL)methyl)formamide

There total 3 articles about N-((6-Methylpyridin-2-YL)methyl)formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

2-aminomethyl-6-methylpyridine (6627-60-7) + formic acid (64-18-6) → N-((6-methylpyridin-2-yl)methyl)formamide (54384-88-2)

Guidance literature:

at 0 - 100 ℃;

Reference yield:

2-Cyano-6-methylpyridine (1620-75-3) → N-((6-methylpyridin-2-yl)methyl)formamide (54384-88-2)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen; palladium 10% on activated carbon / 20 °C / Inert atmosphere

2: 0 - 100 °C

With palladium 10% on activated carbon; hydrogen;

Reference yield:

→ N-((6-methylpyridin-2-yl)methyl)formamide (54384-88-2)

Guidance literature:

entspr. Amin, HCOOH;

DOI:10.1021/jo00897a006

upstream raw materials:

2-aminomethyl-6-methylpyridine

formic acid

2-Cyano-6-methylpyridine

Downstream raw materials:

5-methylimidazo<1,5-a>pyridine

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