3-benzyloxycarbonylaMino-propionic acid dipropylcarbaMoylMethyl ester

Base Information

Chemical Name:3-benzyloxycarbonylaMino-propionic acid dipropylcarbaMoylMethyl ester
CAS No.:1366067-80-2
Molecular Formula:C19H28N2O5
Molecular Weight:364.442
Hs Code.:
Mol file:1366067-80-2.mol

Synonyms:3-benzyloxycarbonylaMino-propionic acid dipropylcarbaMoylMethyl ester

Suppliers and Price of 3-benzyloxycarbonylaMino-propionic acid dipropylcarbaMoylMethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 3-benzyloxycarbonylaMino-propionic acid dipropylcarbaMoylMethyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-benzyloxycarbonylaMino-propionic acid dipropylcarbaMoylMethyl ester

There total 1 articles about 3-benzyloxycarbonylaMino-propionic acid dipropylcarbaMoylMethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2315-37-9
2-chloro-N,N-dipropylacetamide

: 2304-94-1
3-(benzyloxycarbonylamino)propanoic acid

: 1366067-80-2
3-benzyloxycarbonylaminopropionic acid dipropylcarbamoylmethyl ester

Guidance literature:: 3-(benzyloxycarbonylamino)propanoic acid; With sodium carbonate; In N,N-dimethyl-formamide;

2-chloro-N,N-dipropylacetamide; In N,N-dimethyl-formamide; at 60 ℃; for 2.5h;

Reference yield:

: 1366067-80-2
3-benzyloxycarbonylaminopropionic acid dipropylcarbamoylmethyl ester

: 1366295-61-5
3-(3-{2-[(E)-3,5-diamino-6-chloropyrazine-2-carbonylimino]-1,3,8-triazaspiro[4.5]decane-8-carbonyl}benzenesulfonylamino)propionic acid dipropylcarbamoylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: Isopropyl acetate / 20 °C

1.2: 3.5 h

2.1: dmap; 4-methyl-morpholine / water; Isopropyl acetate / 0 °C

2.2: 2 h / 0 - 5 °C

2.3: pH 6

3.1: hydrogen / palladium 10% on activated carbon / Isopropyl acetate / 760.05 - 2280.15 Torr

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 4-methyl-morpholine / water; tetrahydrofuran / 24 h / 20 °C

4.2: 1 h / 20 - 50 °C

5.1: sodium carbonate / dichloromethane; water

With 4-methyl-morpholine; dmap; hydrogen; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; Isopropyl acetate; water;

Reference yield:

: 1366067-80-2
3-benzyloxycarbonylaminopropionic acid dipropylcarbamoylmethyl ester

: 1366067-23-3
3-(2-dipropylcarbamoylmethoxycarbonylethylsulfamoyl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: Isopropyl acetate / 20 °C

1.2: 3.5 h

2.1: dmap; 4-methyl-morpholine / water; Isopropyl acetate / 0 °C

2.2: 2 h / 0 - 5 °C

2.3: pH 6

3.1: hydrogen / palladium 10% on activated carbon / Isopropyl acetate / 760.05 - 2280.15 Torr

With 4-methyl-morpholine; dmap; hydrogen; palladium 10% on activated carbon; In Isopropyl acetate; water;