benzyl 3-(2-dipropylcarbamoylmethoxycarbonylethylsulfamoyl)benzoic acid benzyl ester

Base Information

Chemical Name:benzyl 3-(2-dipropylcarbamoylmethoxycarbonylethylsulfamoyl)benzoic acid benzyl ester
CAS No.:1366067-89-1
Molecular Formula:C₂₅H₃₂N₂O₇S
Molecular Weight:504.604
Hs Code.:

Synonyms:benzyl 3-(2-dipropylcarbamoylmethoxycarbonylethylsulfamoyl)benzoic acid benzyl ester

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Chemical Property of benzyl 3-(2-dipropylcarbamoylmethoxycarbonylethylsulfamoyl)benzoic acid benzyl ester

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Technology Process of benzyl 3-(2-dipropylcarbamoylmethoxycarbonylethylsulfamoyl)benzoic acid benzyl ester

There total 3 articles about benzyl 3-(2-dipropylcarbamoylmethoxycarbonylethylsulfamoyl)benzoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69812-50-6
3-chlorosulfonylbenzoic acid benzyl ester

: 3-aminopropionic acid dipropylcarbamoylmethyl ester trifluoroacetate

: 1366067-89-1
benzyl 3-(2-dipropylcarbamoylmethoxycarbonylethylsulfamoyl)benzoic acid benzyl ester

Guidance literature:: 3-aminopropionic acid dipropylcarbamoylmethyl ester trifluoroacetate; With 4-methyl-morpholine; dmap; In Isopropyl acetate; water; at 0 ℃;

3-chlorosulfonylbenzoic acid benzyl ester; In Isopropyl acetate; at 0 - 5 ℃; for 2h;

With hydrogenchloride; In Isopropyl acetate; water; pH=6;

Reference yield:

: 2315-37-9
2-chloro-N,N-dipropylacetamide

: 1366067-89-1
benzyl 3-(2-dipropylcarbamoylmethoxycarbonylethylsulfamoyl)benzoic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / N,N-dimethyl-formamide

1.2: 2.5 h / 60 °C

2.1: Isopropyl acetate / 20 °C

2.2: 3.5 h

3.1: dmap; 4-methyl-morpholine / water; Isopropyl acetate / 0 °C

3.2: 2 h / 0 - 5 °C

3.3: pH 6

With 4-methyl-morpholine; dmap; sodium carbonate; In Isopropyl acetate; water; N,N-dimethyl-formamide;

Reference yield:

: 1366067-80-2
3-benzyloxycarbonylaminopropionic acid dipropylcarbamoylmethyl ester

: 1366067-89-1
benzyl 3-(2-dipropylcarbamoylmethoxycarbonylethylsulfamoyl)benzoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: Isopropyl acetate / 20 °C

1.2: 3.5 h

2.1: dmap; 4-methyl-morpholine / water; Isopropyl acetate / 0 °C

2.2: 2 h / 0 - 5 °C

2.3: pH 6

With 4-methyl-morpholine; dmap; In Isopropyl acetate; water;