3-(2-(4-chloro-1H-imidazol-1-yl)-5-nitrophenoxy)propan-1-amine

Base Information

Chemical Name:3-(2-(4-chloro-1H-imidazol-1-yl)-5-nitrophenoxy)propan-1-amine
CAS No.:1356009-14-7
Molecular Formula:C₁₂H₁₃ClN₄O₃
Molecular Weight:296.713
Hs Code.:
Mol file:1356009-14-7.mol

Synonyms:3-(2-(4-chloro-1H-imidazol-1-yl)-5-nitrophenoxy)propan-1-amine

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Chemical Property of 3-(2-(4-chloro-1H-imidazol-1-yl)-5-nitrophenoxy)propan-1-amine

Chemical Property:

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Technology Process of 3-(2-(4-chloro-1H-imidazol-1-yl)-5-nitrophenoxy)propan-1-amine

There total 4 articles about 3-(2-(4-chloro-1H-imidazol-1-yl)-5-nitrophenoxy)propan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.78%

: 1356009-16-9
tert-butyl 3-(2-(4-chloro-1H-imidazol-1-yl)-5-nitrophenoxy)propylcarbamate

: 1356009-14-7
3-(2-(4-chloro-1H-imidazol-1-yl)-5-nitrophenoxy)propan-1-amine

Guidance literature:: tert-butyl 3-(2-(4-chloro-1H-imidazol-1-yl)-5-nitrophenoxy)propylcarbamate; With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; at 20 ℃; for 3h;

With sodium hydrogencarbonate;

Reference yield:

: 1009-36-5
2-chloro-5-nitroanisole

: 1356009-14-7
3-(2-(4-chloro-1H-imidazol-1-yl)-5-nitrophenoxy)propan-1-amine

Guidance literature:: Multi-step reaction with 4 steps

1: boron tribromide / dichloromethane / -78 - 4 °C / Inert atmosphere

2: caesium carbonate / tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 18 h / 20 °C

3: potassium hydroxide / dimethyl sulfoxide / 18 h / 90 °C

4: hydrogenchloride / 1,4-dioxane; tetrahydrofuran / 3 h / 20 °C

With hydrogenchloride; boron tribromide; caesium carbonate; potassium hydroxide; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 619-10-3
5-nitro-2-chlorophenol

: 1356009-14-7
3-(2-(4-chloro-1H-imidazol-1-yl)-5-nitrophenoxy)propan-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 18 h / 20 °C

2: potassium hydroxide / dimethyl sulfoxide / 18 h / 90 °C

3: hydrogenchloride / 1,4-dioxane; tetrahydrofuran / 3 h / 20 °C

With hydrogenchloride; caesium carbonate; potassium hydroxide; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; 1,4-dioxane; dimethyl sulfoxide; N,N-dimethyl-formamide;