4-Bromo-2,6-diacetylpyridine

Base Information

Chemical Name:4-Bromo-2,6-diacetylpyridine
CAS No.:1393570-07-4
Molecular Formula:
Molecular Weight:242.07
Hs Code.:
Mol file:1393570-07-4.mol

Synonyms:4-Bromo-2,6-diacetylpyridine

Suppliers and Price of 4-Bromo-2,6-diacetylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Atlantic Research Chemicals
1,1''-(4-Bromo-2,6-pyridinediyl)diethanone 95%
1gm:
$ 618.55

Total 7 raw suppliers

Chemical Property of 4-Bromo-2,6-diacetylpyridine

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

1,1''-(4-Bromo-2,6-pyridinediyl)diethanone 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-Bromo-2,6-diacetylpyridine

There total 9 articles about 4-Bromo-2,6-diacetylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1422463-81-7
4-bromo-2,6-bis(1-pyrrolidinylcarbonyl)pyridine

: 676-58-4
methylmagnesium chloride

: 1393570-07-4
1,1’-(4-bromopyridine-2,6-diyl)diethanone

Guidance literature:: 4-bromo-2,6-bis(1-pyrrolidinylcarbonyl)pyridine; methylmagnesium chloride; In tetrahydrofuran; at 0 - 20 ℃; for 1.5h;

With hydrogenchloride; In tetrahydrofuran; water; at 0 ℃;
DOI:10.1016/j.tetlet.2012.11.004

Reference yield: 31.1%

: 1120-87-2
4-bromopyridin

: 127-17-3
2-oxo-propionic acid

: 1393570-07-4
1,1’-(4-bromopyridine-2,6-diyl)diethanone

Guidance literature:: With ammonium peroxydisulfate; sulfuric acid; silver nitrate; In water; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jacs.0c09357

Reference yield:

: 2033-24-1
cycl-isopropylidene malonate

: 206647-42-9
4-bromo-2,6-pyridinedicarboxylic acid chloride

: 1393570-07-4
1,1’-(4-bromopyridine-2,6-diyl)diethanone

Guidance literature:: cycl-isopropylidene malonate; 4-bromo-2,6-pyridinedicarboxylic acid chloride; With pyridine; In dichloromethane; at 0 - 20 ℃; for 18h;

With hydrogenchloride; In water; at 0 ℃; for 0.0833333h;

With acetic acid; In water; at 115 ℃; for 18h;