Technology Process of 7-p-Toluenesulfonylhydrazide Cholesterol 3-Acetate
There total 8 articles about 7-p-Toluenesulfonylhydrazide Cholesterol 3-Acetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Tau;
In
methanol; cyclohexane; water;
at 50 ℃;
for 18h;
Reagent/catalyst;
Solvent;
Temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap / cyclohexane; Petroleum ether / 55 °C / Large scale
2: tetrabutylammomium bromide; tert.-butylhydroperoxide / 8 h / 45 - 50 °C / Large scale
3: hydrogenchloride / methanol / 3 h / 65 °C / Reflux; Large scale
With
hydrogenchloride; tert.-butylhydroperoxide; dmap; tetrabutylammomium bromide;
In
methanol; cyclohexane; Petroleum ether;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutylammomium bromide; tert.-butylhydroperoxide / 8 h / 45 - 50 °C / Large scale
2: hydrogenchloride / methanol / 3 h / 65 °C / Reflux; Large scale
With
hydrogenchloride; tert.-butylhydroperoxide; tetrabutylammomium bromide;
In
methanol;