Technology Process of 2-HYDRAZINO-BENZONITRILE HYDROCHLORIDE
There total 1 articles about 2-HYDRAZINO-BENZONITRILE HYDROCHLORIDE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
anthranilic acid nitrile;
With
hydrogenchloride; sodium nitrate; sodium nitrite;
In
water;
at -7 - -3 ℃;
Cooling with ice;
With
hydrogenchloride; tin(ll) chloride;
In
water;
at -5 ℃;
for 2h;
- Guidance literature:
-
With
sodium methylate;
In
methanol;
for 6.16667h;
Reflux;