1,3-Dioxolane-4-propanol,gamma,5-diethyl-2,2-dimethyl-,(gammaS,4S,5S)-(9CI)

Base Information

Chemical Name:1,3-Dioxolane-4-propanol,gamma,5-diethyl-2,2-dimethyl-,(gammaS,4S,5S)-(9CI)
CAS No.:460076-96-4
Molecular Formula:C12H24O3
Molecular Weight:216.32
Hs Code.:
Mol file:460076-96-4.mol

Synonyms:1,3-Dioxolane-4-propanol,gamma,5-diethyl-2,2-dimethyl-,(gammaS,4S,5S)-(9CI)

Suppliers and Price of 1,3-Dioxolane-4-propanol,gamma,5-diethyl-2,2-dimethyl-,(gammaS,4S,5S)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,3-Dioxolane-4-propanol,gamma,5-diethyl-2,2-dimethyl-,(gammaS,4S,5S)-(9CI)

Chemical Property:

PSA：38.69000
LogP:2.32510

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-Dioxolane-4-propanol,gamma,5-diethyl-2,2-dimethyl-,(gammaS,4S,5S)-(9CI)

There total 5 articles about 1,3-Dioxolane-4-propanol,gamma,5-diethyl-2,2-dimethyl-,(gammaS,4S,5S)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 77-76-9
2,2-dimethoxy-propane

: (3S,4S,5S)-3-Ethyl-heptane-1,4,5-triol

: 460076-96-4
(S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentan-1-ol

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jo101224w

Reference yield:

: 1576-87-0
trans-2-pentenal

: 460076-96-4
(S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentan-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / diethyl ether

2: 68 percent / H⁺ / Heating

3: AD mix-α; CH3SO2NH2 / 48 h

4: LAH / diethyl ether

5: PTSA

With AD-mix-α; lithium aluminium tetrahydride; methanesulfonamide; hydrogen cation; toluene-4-sulfonic acid; In diethyl ether; 3: Claisen rearrangement Johnson variant;
DOI:10.1021/ja026728s

Reference yield:

: 35077-65-7
(+/-)-(E)-hept-4-en-3-ol

: 460076-96-4
(S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 68 percent / H⁺ / Heating

2: AD mix-α; CH3SO2NH2 / 48 h

3: LAH / diethyl ether

4: PTSA

With AD-mix-α; lithium aluminium tetrahydride; methanesulfonamide; hydrogen cation; toluene-4-sulfonic acid; In diethyl ether; 2: Claisen rearrangement Johnson variant;
DOI:10.1021/ja026728s