N-tert-Amyl-1,1-dimethylallylamine

Base Information

Chemical Name:N-tert-Amyl-1,1-dimethylallylamine
CAS No.:2978-45-2
Molecular Formula:C2H5C(CH3)2NHC(CH3)2CH=CH2
Molecular Weight:155.28
Hs Code.:2921199090
European Community (EC) Number:631-105-5
DSSTox Substance ID:DTXSID80395108
Wikidata:Q82194944
Mol file:2978-45-2.mol

Synonyms:N-tert-Amyl-1,1-dimethylallylamine;2978-45-2;2-methyl-N-(2-methylbut-3-en-2-yl)butan-2-amine;2-Methyl-N-(tert-pentyl)but-3-en-2-amine;starbld0045409;SCHEMBL479720;DTXSID80395108;N-TERT-AMYL-1,1-DIMETHYLALLYLAMINE, 97%;J-017638;(2-METHYLBUT-3-EN-2-YL)(2-METHYLBUTAN-2-YL)AMINE

Suppliers and Price of N-tert-Amyl-1,1-dimethylallylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-TERT-AMYL-1,1-DIMETHYLALLYLAMINE 95.00%
5G
$ 1006.58

Total 5 raw suppliers

Chemical Property of N-tert-Amyl-1,1-dimethylallylamine

Chemical Property:

Refractive Index:n20/D 1.4395(lit.)
Boiling Point:168oC(lit.)
Flash Point:105 °F
PSA：12.03000
Density:0.793 g/mL at 25oC(lit.)
LogP:3.12010
XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:155.167399674
Heavy Atom Count:11
Complexity:134

Purity/Quality:

99% ^*data from raw suppliers

N-TERT-AMYL-1,1-DIMETHYLALLYLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:C
Statements: 10-34
Safety Statements: 26-36/37/39-45

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(C)(C)NC(C)(C)C=C

Technology Process of N-tert-Amyl-1,1-dimethylallylamine

There total 5 articles about N-tert-Amyl-1,1-dimethylallylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 2978-40-7
3-tert.-Amylamino-3-methyl-1-butin

: 2978-45-2
3-Methyl-3-tert-pentylamino-1-butene

Guidance literature:: With hydrogen; Lindlar's catalyst; In various solvent(s); at -10 ℃; under 2585.74 Torr;
DOI:10.1515/znb-2000-0118

Reference yield:

: 1111-97-3
3-chloro-3-methylbut-1-yne

: 2978-45-2
3-Methyl-3-tert-pentylamino-1-butene

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / cuprous chloride; copper bronze; H₂O / 2 h / 25 - 35 °C

2: 83 percent / H₂ / Lindlar catalyst / various solvent(s) / -10 °C / 2585.74 Torr

With water; hydrogen; copper; copper(l) chloride; Lindlar's catalyst; In various solvent(s); 1: Alkylation / 2: Catalytic hydrogenation;
DOI:10.1515/znb-2000-0118

Reference yield:

: 2978-58-7
1,1-dimethylprop-3-ynylamine

: 2978-45-2
3-Methyl-3-tert-pentylamino-1-butene

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Raney-Ni / ethanol

2: Cu, aq. KOH

3: Na, liq. NH₃, NH₄Cl

With potassium hydroxide; ammonia; hydrogen; sodium; copper; ammonium chloride; nickel; In ethanol;
DOI:10.1021/jo01019a033