1-[3-O,5-O-Bis(4-methylbenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl]-2(1H)-pyridinone

Base Information

Chemical Name:1-[3-O,5-O-Bis(4-methylbenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl]-2(1H)-pyridinone
CAS No.:24616-99-7
Molecular Formula:C26H25NO6
Molecular Weight:447.48
Hs Code.:
Mol file:24616-99-7.mol

Synonyms:1-[3-O,5-O-Bis(4-methylbenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl]-2(1H)-pyridinone

Suppliers and Price of 1-[3-O,5-O-Bis(4-methylbenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl]-2(1H)-pyridinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-[3-O,5-O-Bis(4-methylbenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl]-2(1H)-pyridinone

Chemical Property:

Melting Point:159 °C
PSA：83.83000
LogP:3.83520

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 1-[3-O,5-O-Bis(4-methylbenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl]-2(1H)-pyridinone

There total 6 articles about 1-[3-O,5-O-Bis(4-methylbenzoyl)-2-deoxy-α-D-erythro-pentofuranosyl]-2(1H)-pyridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 142-08-5,1199357-22-6
2-Pyridone

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 24616-98-6
2-<2'-deoxy-3',5'-di-O-(p-toluoyl)-β-D-erythro-pentofuranosyloxy>pyridine

: 24617-00-3
1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-β-D-erythro-pentofuranosyl>-2(1H)-pyridone

: 24616-99-7
1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyridone

Guidance literature:: With sodium hydride; In acetonitrile; Product distribution; Ambient temperature; also with other reagents, solvents, times and temp.; glycosylation reactions;

Reference yield: 45.0%

: 24616-98-6
2-<2'-deoxy-3',5'-di-O-(p-toluoyl)-β-D-erythro-pentofuranosyloxy>pyridine

: 24617-00-3
1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-β-D-erythro-pentofuranosyl>-2(1H)-pyridone

: 24616-99-7
1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyridone

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; at 65 ℃; for 4h;

Reference yield:

: 142-08-5,1199357-22-6
2-Pyridone

: 24616-99-7
1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyridone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) KOH / 1) CH₃CN, 5 min, room temp.; 2) 10 min, room temp.

2: 45 percent / p-CH₃C₆H₄SO₃H / acetonitrile / 4 h / 65 °C

With potassium hydroxide; toluene-4-sulfonic acid; In acetonitrile;