3H-3-BENZAZEPINE-3-CARBOXYLIC ACID, 1,2,4,5-TETRAHYDRO-7-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-, 1,1-DIMETHYLETHYL ESTER

Base Information

Chemical Name:3H-3-BENZAZEPINE-3-CARBOXYLIC ACID, 1,2,4,5-TETRAHYDRO-7-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-, 1,1-DIMETHYLETHYL ESTER
CAS No.:720692-76-2
Molecular Formula:C21H32BNO4
Molecular Weight:373.3
Hs Code.:
Mol file:720692-76-2.mol

Synonyms:3H-3-BENZAZEPINE-3-CARBOXYLIC ACID, 1,2,4,5-TETRAHYDRO-7-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-, 1,1-DIMETHYLETHYL ESTER

Suppliers and Price of 3H-3-BENZAZEPINE-3-CARBOXYLIC ACID, 1,2,4,5-TETRAHYDRO-7-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-, 1,1-DIMETHYLETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,2,4,5-TETRAHYDRO-7-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-3H-3-BENZAZEPINE-3-CARBOXYLIC ACID-1,1-DIMETHYLETHYL ESTER 95.00%
5MG
$ 502.44

Total 5 raw suppliers

Chemical Property of 3H-3-BENZAZEPINE-3-CARBOXYLIC ACID, 1,2,4,5-TETRAHYDRO-7-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-, 1,1-DIMETHYLETHYL ESTER

Chemical Property:

PSA：48.00000
LogP:3.25940

Purity/Quality:

97% ^*data from raw suppliers

1,2,4,5-TETRAHYDRO-7-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-3H-3-BENZAZEPINE-3-CARBOXYLIC ACID-1,1-DIMETHYLETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3H-3-BENZAZEPINE-3-CARBOXYLIC ACID, 1,2,4,5-TETRAHYDRO-7-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-, 1,1-DIMETHYLETHYL ESTER

There total 1 articles about 3H-3-BENZAZEPINE-3-CARBOXYLIC ACID, 1,2,4,5-TETRAHYDRO-7-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-, 1,1-DIMETHYLETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 73183-34-3
bis(pinacol)diborane

: 264264-28-0
1,1-dimethylethyl-7-{[(trifluoromethyl)sulfonyl]oxy}-1,2,4,5-tetrahydro-3H-3-benzazepine-3-carboxylate

: 720692-76-2
t-butyl 7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylate

Guidance literature:: With potassium acetate; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 80 ℃; for 3h; Inert atmosphere;

Reference yield: 88.0%

: 5-(5-bromo-1,3,4-thiadiazol-2-yl)-2-[(1-methylethyl)oxy]-benzonitrile

: 720692-76-2
t-butyl 7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylate

: 1258440-68-4
1,1-dimethylethyl 7-(5-{3-cyano-4-[(1-methylethyl)oxy]phenyl}-1,3,4-thiadiazol-2-yl)-1,2,4,5-tetrahydro-3H-3-benzazepine-3-carboxylate

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 120 ℃; for 0.333333h; Microwave irradiation;

Reference yield: 69.0%

: 720692-76-2
t-butyl 7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylate

: 1258440-40-2
5-bromo-2-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,3-thiazole

: 1258440-42-4
1,1-dimethylethyl 7-(2-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,3-thiazol-5-yl)-1,2,4,5-tetrahydro-3H-3-benzazepine-3-carboxylate

Guidance literature:: With sodium hydrogencarbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; water; at 90 ℃; for 2h; Inert atmosphere;