(2-Methylphenyl)(2,4,6-triMethylphenyl)iodoniuM triflate

Base Information

• Chemical Name: (2-Methylphenyl)(2,4,6-triMethylphenyl)iodoniuM triflate
• CAS No.: 210823-54-4
• Molecular Formula: CF₃O₃S*C₁₆H₁₈I
• Molecular Weight: 486.294
• Hs Code.: 2902909090
• Mol file: 210823-54-4.mol

Synonyms:(2-Methylphenyl)(2,4,6-triMethylphenyl)iodoniuM triflate;(2-Methylphenyl)(2,4,6-trimethylphenyl)iodonium trifluoromethanesulfonate;Mesityl(o-tolyl)iodonium triflate

Chemical Property of (2-Methylphenyl)(2,4,6-triMethylphenyl)iodoniuM triflate

Chemical Property:

• Melting Point: 166.0 to 170.0 °C
• PSA: 65.58000
• LogP: 2.18080
• Solubility.: soluble in Methanol

Purity/Quality:

99%, ^*data from raw suppliers

(2-Methylphenyl)(2,4,6-trimethylphenyl)iodonium Trifluoromethanesulfonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): 7965987
• Hazard Codes: T
• Statements: 25-36/37/38
• Safety Statements: 26-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2-Methylphenyl)(2,4,6-triMethylphenyl)iodoniuM triflate

There total 1 articles about (2-Methylphenyl)(2,4,6-triMethylphenyl)iodoniuM triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

ortho-methylphenyl iodide (615-37-2) + trifluorormethanesulfonic acid (1493-13-6) + 1,3,5-trimethyl-benzene (108-67-8) → 2-methylphenyl(mesityl)iodonium trifluoromethanesulfonate (210823-54-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 2.08333h;

DOI:10.1021/ol402600r

Reference yield: 69.0%

1-phenylethyl cyanide (1823-91-2) + 2-methylphenyl(mesityl)iodonium trifluoromethanesulfonate (210823-54-4) → 2-phenyl-N-(o-tolyl)propanamide (59960-38-2)

Guidance literature:

With copper (I) trifluoromethane sulfonate toluene complex; caesium carbonate; In toluene; at 80 ℃; for 0.333333h;

DOI:10.1039/d1ra02305e

Reference yield: 53.0%

2-methylphenyl(mesityl)iodonium trifluoromethanesulfonate (210823-54-4) + 2-acetamidobenzonitrile (25116-00-1) → (Z)-2-methyl-N-(2-methyl-4H-benzo[d][1,3]oxazin-4-ylidene)aniline

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); In 1,2-dichloro-ethane; at 75 ℃; Inert atmosphere;

DOI:10.1002/adsc.201400763

upstream raw materials:

ortho-methylphenyl iodide

trifluorormethanesulfonic acid

1,3,5-trimethyl-benzene

Downstream raw materials:

2-methyl-6-(4-methylpyridin-1-ium-1-yl)phenolate

2-phenyl-N-(o-tolyl)propanamide

2-(2-methylphenyl)-1-phenyl-1-ethanone

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