7,8-Dibromo-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane

Base Information

• Chemical Name: 7,8-Dibromo-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane
• CAS No.: 51249-62-8
• Molecular Formula: C8H3Br2F13
• Molecular Weight: 505.8966616
• Hs Code.: 2903793090
• Mol file: 51249-62-8.mol

Synonyms:7,8-Dibromo-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane;1,2-Dibromo-1-(perfluoro-n-hexyl)ethane

Chemical Property of 7,8-Dibromo-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane

Chemical Property:

• PSA: 0.00000
• LogP: 5.88360

Purity/Quality:

99%min. ^*data from raw suppliers

1,2-Dibromo-1-(perfluoro-n-hexyl)ethane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7,8-Dibromo-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane

There total 3 articles about 7,8-Dibromo-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene (25291-17-2) → 1,2-Dibrom-1H,1H,2H-perfluorooctane (51249-62-8)

Guidance literature:

With bromine; at 120 ℃; for 5h; Irradiation;

DOI:10.1016/S0022-1139(00)00319-5

Reference yield:

methanol (67-56-1) + 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene (25291-17-2) → 1,2-Dibrom-1H,1H,2H-perfluorooctane (51249-62-8) + 2-Bromo-1-methoxy-1H,1H,2H-perfluorooctane

Guidance literature:

With bromine; oxygen; mercury(II) sulfate; In dichloromethane; for 120h; Title compound not separated from byproducts;

DOI:10.1016/S0022-1139(00)00319-5

Reference yield:

3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene (25291-17-2) → 1,2-Dibrom-1H,1H,2H-perfluorooctane (51249-62-8) + 1-Bromo-2-chloro-1H,1H,2H-perfluorooctane + 1,2-Dichloro-1H,1H,2H-perfluorooctane + 2-Bromo-1-chloro-1H,1H,2H-perfluorooctane

Guidance literature:

With bromine chloride; at 0 ℃; for 0.333333h; Title compound not separated from byproducts; Irradiation;

DOI:10.1016/S0022-1139(00)00319-5

upstream raw materials:

3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene

methanol

Downstream raw materials:

2-F-Hexyl-2-brom-aethen

7H,8H-hexacosafluoro-tetradec-7-ene