3,5-BIS(TRIFLUOROMETHYL)PHENYLTHIOETHANOL

Base Information

Chemical Name:3,5-BIS(TRIFLUOROMETHYL)PHENYLTHIOETHANOL
CAS No.:450409-97-9
Molecular Formula:C10H8F6OS
Molecular Weight:290.23
Hs Code.:2930909090
Mol file:450409-97-9.mol

Synonyms:3,5-BIS(TRIFLUOROMETHYL)PHENYLTHIOETHANOL

Suppliers and Price of 3,5-BIS(TRIFLUOROMETHYL)PHENYLTHIOETHANOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3,5-BIS(TRIFLUOROMETHYL)PHENYLTHIOETHANOL 98.00%
25G
$ 1697.85

AHH
3,5-Bis(trifluoromethyl)phenylthioethanol 98%
25g
$ 310.00

Total 3 raw suppliers

Chemical Property of 3,5-BIS(TRIFLUOROMETHYL)PHENYLTHIOETHANOL

Chemical Property:

PSA：45.53000
LogP:3.80860

Purity/Quality:

99% ^*data from raw suppliers

3,5-BIS(TRIFLUOROMETHYL)PHENYLTHIOETHANOL 98.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,5-BIS(TRIFLUOROMETHYL)PHENYLTHIOETHANOL

There total 1 articles about 3,5-BIS(TRIFLUOROMETHYL)PHENYLTHIOETHANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 130783-02-7
3,5-bis(trifluoromethyl)thiophenol

: 540-51-2
2-bromoethanol

: 450409-97-9
2-[3,5-di(trifluoromethyl)phenylsulfanyl]-1-ethanol

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 24h;
DOI:10.1055/s-2003-36844

Reference yield:

: 450409-97-9
2-[3,5-di(trifluoromethyl)phenylsulfanyl]-1-ethanol

: 450409-87-7
2-[3,5-bis(trifluoromethyl)phenylsulfonyl]-1-ethanol

Guidance literature:: With manganese(II) sulfate; dihydrogen peroxide; sodium hydrogencarbonate; In water; acetonitrile; at 20 ℃; for 0.25h;
DOI:10.1016/S0040-4039(02)00598-1

Reference yield:

: 450409-97-9
2-[3,5-di(trifluoromethyl)phenylsulfanyl]-1-ethanol

: 548740-06-3
3,5-bis(trifluoromethyl)phenyl vinyl sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: MnSO₄; aq. H₂O₂; NaHCO₃ / acetonitrile / 20 °C

2: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; DMAP / CH₂Cl₂ / 12 h / 20 °C

3: aq. NaHCO₃ / acetone / 12 h / 20 °C

With dmap; manganese(II) sulfate; dihydrogen peroxide; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; acetone; acetonitrile;
DOI:10.1055/s-2003-36844