Ethyl 2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate

Base Information

Chemical Name:Ethyl 2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate
CAS No.:19620-33-8
Molecular Formula:C13H20O4
Molecular Weight:240.2955
Hs Code.:2932999099
DSSTox Substance ID:DTXSID50575475
Mol file:19620-33-8.mol

Synonyms:ethyl 2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate;19620-33-8;ethyl 2-{1,4-dioxaspiro[4.5]decan-8-ylidene}propanoate;LNZFOEZRSXUJFJ-UHFFFAOYSA-N;SCHEMBL1189435;Ethyl2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate;DTXSID50575475;AC5143;MFCD22681615;AKOS016845028;SY130799;CS-0449126;J-520569

Suppliers and Price of Ethyl 2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Ethyl2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate 95+%
1g
$ 772.00

Chemenu
ethyl2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate 95%
1g
$ 729.00

American Custom Chemicals Corporation
ETHYL-2-(1,4-DIOXASPIRO[4.5]DECAN-8-YLIDENE)PROPANOATE 95.00%
5MG
$ 504.74

Alichem
Ethyl2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate
1g
$ 646.84

AK Scientific
Ethyl2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate
1g
$ 802.00

Total 7 raw suppliers

Chemical Property of Ethyl 2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate

Chemical Property:

PSA：44.76000
LogP:2.18310
Storage Temp.:2-8°C
XLogP3:1.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:240.13615911
Heavy Atom Count:17
Complexity:314

Purity/Quality:

97% ^*data from raw suppliers

Ethyl2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=C1CCC2(CC1)OCCO2)C

Technology Process of Ethyl 2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate

There total 6 articles about Ethyl 2-(1,4-dioxaspiro[4.5]decan-8-ylidene)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 31180-83-3
2-(4-oxocyclohexylidene)propanoic acid ethyl ester

: 107-21-1
ethylene glycol

: 19620-33-8
ethyl 2-(4,4-ethylenedioxycyclohex-1-ylidene)propionate

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 4h; Heating;
DOI:10.1016/j.tetlet.2007.07.163 DOI:10.1016/j.tet.2008.08.095

Reference yield: 86.0%

: 19620-33-8
ethyl 2-(4,4-ethylenedioxycyclohex-1-ylidene)propionate

Guidance literature:

Reference yield: 78.0%

: 4746-97-8
cyclohexanedione monoethylene ketal

: 3699-66-9
ethyl 2-diethoxyphosphorylpropionate

: 19620-33-8
ethyl 2-(4,4-ethylenedioxycyclohex-1-ylidene)propionate

Guidance literature:: ethyl 2-diethoxyphosphorylpropionate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

cyclohexanedione monoethylene ketal; In tetrahydrofuran; at 0 ℃; for 2h;