1,3,2-Dioxaborolane, 2-[(1E)-2-(3-fluorophenyl)ethenyl]-4,4,5,5-tetramethyl-

Base Information

Chemical Name:1,3,2-Dioxaborolane, 2-[(1E)-2-(3-fluorophenyl)ethenyl]-4,4,5,5-tetramethyl-
CAS No.:633327-36-3
Molecular Formula:C14H18BFO2
Molecular Weight:248.105
Hs Code.:2934999090

Synonyms:1,3,2-Dioxaborolane, 2-[(1E)-2-(3-fluorophenyl)ethenyl]-4,4,5,5-tetramethyl-

Suppliers and Price of 1,3,2-Dioxaborolane, 2-[(1E)-2-(3-fluorophenyl)ethenyl]-4,4,5,5-tetramethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Atlantic Research Chemicals
2-[2-(3-Fluorophenyl)ethenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95%
1gm:
$ 703.38

Total 3 raw suppliers

Chemical Property of 1,3,2-Dioxaborolane, 2-[(1E)-2-(3-fluorophenyl)ethenyl]-4,4,5,5-tetramethyl-

Chemical Property:

PSA：18.46000
LogP:3.47030

Purity/Quality:

95% ^*data from raw suppliers

2-[2-(3-Fluorophenyl)ethenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3,2-Dioxaborolane, 2-[(1E)-2-(3-fluorophenyl)ethenyl]-4,4,5,5-tetramethyl-

There total 6 articles about 1,3,2-Dioxaborolane, 2-[(1E)-2-(3-fluorophenyl)ethenyl]-4,4,5,5-tetramethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 350-51-6
3-fluorostyrene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 633327-36-3
(E)-2-(3-fluorostyryl)-4,4,5,5-tetramethyl-1,3-dioxa-2-borolane

Guidance literature:: With bis(cyclopentadienyl)dihydrozirconium; In toluene; at 25 ℃; Inert atmosphere; Glovebox;
DOI:10.1002/anie.201908931

Reference yield: 88.0%

: 2561-17-3
1-ethynyl-3-fluoro-benzene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 633327-36-3
(E)-2-(3-fluorostyryl)-4,4,5,5-tetramethyl-1,3-dioxa-2-borolane

Guidance literature:: With tris(bis(trimethylsilyl)amido)lanthanum(III); In neat (no solvent); at 60 ℃; for 24h;
DOI:10.1002/cjoc.201900344

Reference yield: 82.0%

: 705-83-9
3-(m-fluorophenyl)-propiolic acid

: 73183-34-3
bis(pinacol)diborane

: 633327-36-3
(E)-2-(3-fluorostyryl)-4,4,5,5-tetramethyl-1,3-dioxa-2-borolane

Guidance literature:: With copper(II) trifluoroacetate; sodium carbonate; In 1,4-dioxane; at 80 ℃; for 18h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.cclet.2016.02.012