Hydrazinecarboxylic acid, (tetrahydro-4H-pyran-4-ylidene)-, 1,1-dimethylethyl

Base Information

• Chemical Name: Hydrazinecarboxylic acid, (tetrahydro-4H-pyran-4-ylidene)-, 1,1-dimethylethyl
• CAS No.: 693287-78-4
• Molecular Formula: C10H18N2O3
• Molecular Weight: 214.26152
• Mol file: 693287-78-4.mol

Synonyms:Hydrazinecarboxylic acid, (tetrahydro-4H-pyran-4-ylidene)-, 1,1-dimethylethyl;2-(Tetrahydro-4H-pyran-4-ylidene)hydrazinecarboxylic acid 1,1-dimethylethyl ester;N'-(Tetrahydropyran-4-ylidene)hydrazinecarboxylic acid tert-butyl ester;t-Butyl 2(2H-pyran-4(3H,5H,6H)-ylidene)hydrazinecarboxylate

Chemical Property of Hydrazinecarboxylic acid, (tetrahydro-4H-pyran-4-ylidene)-, 1,1-dimethylethyl

Chemical Property:

• PSA: 59.92000
• Density: 1.14
• LogP: 2.06840

Purity/Quality:

99% ^*data from raw suppliers

t-Butyl2(2H-Pyran-4(3H,5H,6H)-ylidene)hydrazinecarboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hydrazinecarboxylic acid, (tetrahydro-4H-pyran-4-ylidene)-, 1,1-dimethylethyl

There total 2 articles about Hydrazinecarboxylic acid, (tetrahydro-4H-pyran-4-ylidene)-, 1,1-dimethylethyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Tetrahydro-4H-pyran-4-one (29943-42-8,143562-54-3) + t-butoxycarbonylhydrazine (870-46-2) → N’-(tetrahydropyran-4-ylidene)hydrazinecarboxylic acid tert-butyl ester (693287-78-4)

Guidance literature:

In methanol; at 20 ℃;

DOI:10.1021/jm030276s

Reference yield:

→ N’-(tetrahydropyran-4-ylidene)hydrazinecarboxylic acid tert-butyl ester (693287-78-4)

Guidance literature:

Reference yield: 100.0%

N’-(tetrahydropyran-4-ylidene)hydrazinecarboxylic acid tert-butyl ester (693287-78-4) → N’-(tetrahydropyran-4-yl)hydrazinecarboxylic acid tert-butyl ester (693287-79-5)

Guidance literature:

With sodium cyanoborohydride; acetic acid; at 20 ℃;

DOI:10.1021/jm030276s

upstream raw materials:

Tetrahydro-4H-pyran-4-one

t-butoxycarbonylhydrazine

Downstream raw materials:

N’-(tetrahydropyran-4-yl)hydrazinecarboxylic acid tert-butyl ester

tetrahydro-2H-pyran-4-yl-hydrazine

methyl 5-(4-methylthiophenyl)-1-(tetrahydro-2H-pyran-4-yl)pyrazole-3-carboxylate

[5-(4-methanesulfonyl-phenyl)-1-(tetrahydro-pyran-4-yl)-1H-pyrazol-3-yl]-methanol

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