tert-butyl 5-(((4-nitrophenoxy)carbonyloxy)methyl)-1H-imidazole-1-carboxylate

Base Information

• Chemical Name: tert-butyl 5-(((4-nitrophenoxy)carbonyloxy)methyl)-1H-imidazole-1-carboxylate
• CAS No.: 1401248-97-2
• Molecular Formula: C₁₆H₁₇N₃O₇
• Molecular Weight: 363.327
• Mol file: 1401248-97-2.mol

Synonyms:tert-butyl 5-(((4-nitrophenoxy)carbonyloxy)methyl)-1H-imidazole-1-carboxylate

Chemical Property of tert-butyl 5-(((4-nitrophenoxy)carbonyloxy)methyl)-1H-imidazole-1-carboxylate

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Technology Process of tert-butyl 5-(((4-nitrophenoxy)carbonyloxy)methyl)-1H-imidazole-1-carboxylate

There total 2 articles about tert-butyl 5-(((4-nitrophenoxy)carbonyloxy)methyl)-1H-imidazole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis-(p-nitrophenyl) carbonate (5070-13-3) + tert-butyl 5-(hydroxymethyl)-1H-imidazole-1-carboxylate → tert-butyl 5-(((4-nitrophenoxy)carbonyloxy)methyl)-1H-imidazole-1-carboxylate (1401248-97-2)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1021/jm400288z

Reference yield:

4-Nitrophenyl chloroformate (7693-46-1) + tert-butyl 5-(hydroxymethyl)-1H-imidazole-1-carboxylate → tert-butyl 5-(((4-nitrophenoxy)carbonyloxy)methyl)-1H-imidazole-1-carboxylate (1401248-97-2)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1021/jm400288z

Reference yield:

(S)-N-((2R,5R)-5-amino-1,6-diphenylhexan-2-yl)-2-(3-((2-isopropylthiazol-4-yl)methyl)-3-methylureido)-3-methylbutanamide hydrochloride (1383570-58-8) + tert-butyl 5-(((4-nitrophenoxy)carbonyloxy)methyl)-1H-imidazole-1-carboxylate (1401248-97-2) → tert-butyl 5-((5S,8R,11R)-8,11-dibenzyl-5-isopropyl-1-(2-isopropylthiazol-4-yl)-2-methyl-3,6,13-trioxo-14-oxa-2,4,7,12-tetraazapentadecan-15-yl)-1H-imidazole-1-carboxylate (1383570-60-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 16h;

DOI:10.1021/jm400288z

upstream raw materials:

bis-(p-nitrophenyl) carbonate

4-Nitrophenyl chloroformate

Downstream raw materials:

tert-butyl 5-((5S,8R,11R)-8,11-dibenzyl-5-isopropyl-1-(2-isopropylthiazol-4-yl)-2-methyl-3,6,13-trioxo-14-oxa-2,4,7,12-tetraazapentadecan-15-yl)-1H-imidazole-1-carboxylate

(1H-imidazol-5-yl)methyl [(2R,5R)-5-((S)-2-(3-((2-isopropylthiazol-4-yl)methyl)-3-methylureido)-3-methylbutanamido)-1,6-diphenylhexan-2-yl]carbamate

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