2-Thiazolidineaceticacid, 4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[5,5-dimethyl-a-[(phenylacetyl)amino]-, dimethylester, (aR,a'R,2R,2'R,4S,4'S)- (9CI)

Base Information

Chemical Name:2-Thiazolidineaceticacid, 4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[5,5-dimethyl-a-[(phenylacetyl)amino]-, dimethylester, (aR,a'R,2R,2'R,4S,4'S)- (9CI)
CAS No.:142780-80-1
Molecular Formula:C36H48 N6 O8 S2
Molecular Weight:756.9317
Hs Code.:

2-Thiazolidineaceticacid, 4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[5,5-dimethyl-a-[(phenylacetyl)amino]-, dimethylester, (aR,a'R,2R,2'R,4S,4'S)- (9CI)

Synonyms:2-Thiazolidineaceticacid, 4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[5,5-dimethyl-a-[(phenylacetyl)amino]-, dimethylester, [2R-[2a(R*),4b[2'R*(R*),4'S*]]]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Thiazolidineaceticacid, 4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[5,5-dimethyl-a-[(phenylacetyl)amino]-, dimethylester, (aR,a'R,2R,2'R,4S,4'S)- (9CI)

Chemical Property:

Boiling Point:1025.4°Cat760mmHg
Flash Point:573.9°C
PSA：257.62000
Density:1.246g/cm³
LogP:4.65800

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Thiazolidineaceticacid, 4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[5,5-dimethyl-a-[(phenylacetyl)amino]-, dimethylester, (aR,a'R,2R,2'R,4S,4'S)- (9CI)

There total 5 articles about 2-Thiazolidineaceticacid, 4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[5,5-dimethyl-a-[(phenylacetyl)amino]-, dimethylester, (aR,a'R,2R,2'R,4S,4'S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 67-56-1
methanol

: 142762-72-9
<2S-<2α,5α,6β>>-N,N'-<1,2-ethanediyl>bis<3,3-dimethyl-7-oxo-6-<(phenylacetyl)amino>-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxamide>

: 142780-80-1
[2R-(2α(R^*),4β)]-4,4'-[1,2-ethanediylbis(aminocarbonyl)]bis[5,5-dimethyl-α-[(phenylacetyl)amino]-2-thiazolidineacetic acid methyl ester]

Guidance literature:: at 21 ℃; for 3h;
DOI:10.1021/jm00073a011

Reference yield:

: 39879-63-5
penicillin-G N-ethylpiperidine salt

: 142780-80-1
[2R-(2α(R^*),4β)]-4,4'-[1,2-ethanediylbis(aminocarbonyl)]bis[5,5-dimethyl-α-[(phenylacetyl)amino]-2-thiazolidineacetic acid methyl ester]

Guidance literature:: Multi-step reaction with 3 steps

1: CHCl₃ / 2 h / -11 °C

2: CHCl₃ / 2 h / 0 - 19 °C

3: 89 percent / 3 h / 21 °C

In chloroform;
DOI:10.1021/jm00073a011

Reference yield:

: 19870-47-4
benzylpenicillin-(carbonic acid ethyl ester)-anhydride

: 142780-80-1
[2R-(2α(R^*),4β)]-4,4'-[1,2-ethanediylbis(aminocarbonyl)]bis[5,5-dimethyl-α-[(phenylacetyl)amino]-2-thiazolidineacetic acid methyl ester]

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃ / 2 h / 0 - 19 °C

2: 89 percent / 3 h / 21 °C

In chloroform;
DOI:10.1021/jm00073a011