SPhos Pd G3

Base Information

• Chemical Name: SPhos Pd G3
• CAS No.: 1445085-82-4
• Molecular Formula: C39H48NO5PPdS
• Molecular Weight: 866.201401
• Mol file: 1445085-82-4.mol

Synonyms:Methanesulfonato(2-dicyclohexylphosphino-2',6'-diMethoxy-1,1'-biphenyl)(2'-aMino-1,1'-biphenyl-2-yl)palladiuM(II) dichloroMethane adduct, Min. 98% [SPhos Palladacycle];Methanesulfonato(2-dicyclohexylphosphino-2',6'-diMethoxy-1,1'-biphenyl)(2'-aMino-1,1'-biphenyl-2-yl)palladiuM(II) dichloroMethane adduct, Min. 98%;(2-Dicyclohexylphosphino-2',6'-dimethoxybiphenyl) [2-(2'-amino-1,1'-biphenyl)]palladium(II) methanesulfonate;Methanesulfonato(2-dicyclohexylphosphino-2',6'-dimethoxy-1,1'-biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II)dichloromethane adduct;[2'-(Amino)[1,1'-biphenyl]-2-yl][dicyclohexyl(2',6'-dimethoxy[1,1'-biphenyl]-2-yl)phosphine](methanesulfonato)palladium;Methanesulfonato(2-dicyclohexylphosphino-2',6'-dimethoxy-1,1'-biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II) dichloromethane adduct OMS-SPhos;SPhos Pd G3 97%

Chemical Property of SPhos Pd G3

Chemical Property:

• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

SPhos Pd G3 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: SPhos Pd G3 is stable phosphine-ligated palladium precatalyst that can be used in the catalysis of C-C and C-N bond formation reactions.

Technology Process of SPhos Pd G3

There total 3 articles about SPhos Pd G3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane (657408-07-6) + (2'-amino-1,1'-biphenyl-2-yl)methanesulfonatopalladium(II) dimer (1435520-65-2) → C26H35O2P*C13H13NO3PdS (1445085-82-4)

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1039/c2sc20903a

Reference yield:

[1,1'-biphenyl]-2-aminium methanesulfonate (1445085-50-6) → C26H35O2P*C13H13NO3PdS (1445085-82-4)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 65 °C

2: tetrahydrofuran / 20 °C

In tetrahydrofuran; toluene;

DOI:10.1039/c2sc20903a

Reference yield:

2-phenylaniline (90-41-5) → C26H35O2P*C13H13NO3PdS (1445085-82-4)

Guidance literature:

Multi-step reaction with 3 steps

1: Isopropyl acetate / 20 °C

2: toluene / 65 °C

3: tetrahydrofuran / 20 °C

In tetrahydrofuran; Isopropyl acetate; toluene;

DOI:10.1039/c2sc20903a

upstream raw materials:

2-phenylaniline

[1,1'-biphenyl]-2-aminium methanesulfonate

dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane

(2'-amino-1,1'-biphenyl-2-yl)methanesulfonatopalladium(II) dimer

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