(1S,2S)-1,2-Bis(4-Methoxyphenyl)ethylenediaMine dihydrochloride

Base Information

Chemical Name:(1S,2S)-1,2-Bis(4-Methoxyphenyl)ethylenediaMine dihydrochloride
CAS No.:820965-96-6
Molecular Formula:C₁₆H₂₀N₂O₂*2ClH
Molecular Weight:345.269
Hs Code.:
Mol file:820965-96-6.mol

Synonyms:(1S,2S)-1,2-Bis(4-methoxyphenyl)ethylenediamine dihydrochloride;(1S,2S)-1,2-Bis(4-methoxyphenyl)-1,2-ethanediamine dihydrochloride;

Suppliers and Price of (1S,2S)-1,2-Bis(4-Methoxyphenyl)ethylenediaMine dihydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
(1S,2S)-1,2-Bis(4-methoxyphenyl)ethylenediamine dihydrochloride 96%
1g
$ 318.00

Sigma-Aldrich
(1S,2S)-1,2-Bis(4-methoxyphenyl)ethylenediamine dihydrochloride 96%
100mg
$ 60.10

American Custom Chemicals Corporation
(1S,2S)-1,2-BIS(4-METHOXYPHENYL)ETHYLENEDIAMINE DIHYDROCHLORIDE 95.00%
1G
$ 915.63

American Custom Chemicals Corporation
(1S,2S)-1,2-BIS(4-METHOXYPHENYL)ETHYLENEDIAMINE DIHYDROCHLORIDE 95.00%
100MG
$ 602.25

Total 2 raw suppliers

Chemical Property of (1S,2S)-1,2-Bis(4-Methoxyphenyl)ethylenediaMine dihydrochloride

Chemical Property:

Melting Point:235-239°C
PSA：70.50000
LogP:5.40820

Purity/Quality:

97% ^*data from raw suppliers

(1S,2S)-1,2-Bis(4-methoxyphenyl)ethylenediamine dihydrochloride 96% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22
Safety Statements: 36/37

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (1S,2S)-1,2-Bis(4-Methoxyphenyl)ethylenediaMine dihydrochloride

There total 1 articles about (1S,2S)-1,2-Bis(4-Methoxyphenyl)ethylenediaMine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 820965-96-6
(1S,2S)-1,2-bis(4-methoxyphenyl)ethylenediamine dihydrogen chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 4 h / Milling

2: hydrogenchloride / water

With hydrogenchloride; In water;

Reference yield:

: 820965-96-6
(1S,2S)-1,2-bis(4-methoxyphenyl)ethylenediamine dihydrogen chloride

: 108-24-7
acetic anhydride

: N-[(1S,2S)-2-Acetylamino-1,2-bis-(4-methoxy-phenyl)-ethyl]-acetamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/ol501143c

Reference yield:

: 820965-96-6
(1S,2S)-1,2-bis(4-methoxyphenyl)ethylenediamine dihydrogen chloride

: 1610353-81-5
(1S,2S)-N,N’-diethyl-1,2-bis(4-methoxyphenyl)ethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 12 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol501143c